NYC 9/11 Public Portal Document
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Data File : C:\HPCHEM\1\DATA\OCT1101\22976.D vial: 7
Acq On : 11 Oct 2001 3:37 pm Operator: 209 GALOS
Sample : reinject Inst : GC/MS 209
Mise Multiplr; 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DAT7kBASE\NBS75K.L
*********************************************************************
Peak Number 1 2-Hexanone Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
6.49 0.74 ug/1 97764 1,4-Dichlorobenzene-d4 11.76
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Hexan' 100 C6H12O 000591-78-6 91
2 2-Hex^ 4-hydroxy-5-methyl-3-pr 172 C10H20O2i 061141-74-0 78
3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 52
4 2-H^anione, 4-hydroxy- 3-propyl- 158 C9H18O2 062338-17-4 40
^bundanc/ Scan 158 (6.491 min); 22976.D (-) m/z 42795 1^0700%
58
5000
T
71 85 6.20 6.40 6.60 6.80
49 m/z
... 58.05 51.09%
•n/z->
Abundance
20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105
#1556: 2-Hexanone
ft
43
58 ................ Z , , I----- - ,
5000
_6,2g^_640__a60__a80^_
m/z ,41.00 15.85%
27 71 85 100
■tI"'!’
nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105
^bundance #15807; 2-Hexanone, 4-hydroxy-5-methyl-3-propyl-
4i3
__a2p__6;4g_a60_jS80^_
5000 m/z SYTOO 15701%
,58
27
72
/85100
■tyrrnT-rrTTp^rf-
..... .. I" " 11 !• > 11 > I' I" " I" " I" " I'"' I,' I"'
Tl/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105
<\bundance #63351; Methyl Isobutyl Ketone
40 _a2o__64g_a6g_a8o__
m/z 100.05 12719%
5000
58
27 85 100
I ' ' ' H ' I' ' I I I I ' I A y \l\ r\iiA
■’T
Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80
22976.D NP091101.M Mon Oct 15 08:40:51 2001 Page 1
NYC-WTC_000087871
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