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GC/MS analysis results for sample AD22976, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22976 conducted on October 15, 2001, identifying unknown compounds.

NYC-WTC_000087863–000087874

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087871
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NYC 9/11 Public Portal Document j-iJ.AJXCiJ.y, OCClXlJll uuilipuuiiu K-epUiL.

Data File : C:\HPCHEM\1\DATA\OCT1101\22976.D vial: 7 Acq On : 11 Oct 2001 3:37 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.74 ug/1 97764 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexan' 100 C6H12O 000591-78-6 91 2 2-Hex^ 4-hydroxy-5-methyl-3-pr 172 C10H20O2i 061141-74-0 78 3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 52 4 2-H^anione, 4-hydroxy- 3-propyl- 158 C9H18O2 062338-17-4 40 ^bundanc/ Scan 158 (6.491 min); 22976.D (-) m/z 42795 1^0700%

58 5000

T 71 85 6.20 6.40 6.60 6.80 49 m/z ... 58.05 51.09% •n/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #1556: 2-Hexanone ft 43

58 ................ Z , , I----- - , 5000 _6,2g^_640__a60__a80^_ m/z ,41.00 15.85% 27 71 85 100 ■tI"'!’ nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ^bundance #15807; 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4i3

__a2p__6;4g_a60_jS80^_ 5000 m/z SYTOO 15701% ,58 27 72 /85100 ■tyrrnT-rrTTp^rf- ..... .. I" " 11 !• > 11 > I' I" " I" " I" " I'"' I,' I"' Tl/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 <\bundance #63351; Methyl Isobutyl Ketone 40 _a2o__64g_a6g_a8o__ m/z 100.05 12719%

5000 58 27 85 100 I ' ' ' H ' I' ' I I I I ' I A y \l\ r\iiA ■’T Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

22976.D NP091101.M Mon Oct 15 08:40:51 2001 Page 1

NYC-WTC_000087871

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NYC-WTC_000087871Source: NYC Law Department, mirrored locally

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