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GC/MS analysis results for sample AD23080, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD23080 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087817–000087841

Folder label: “GC/MS Scan 9/21/01

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• Data' File C:\HPCHEM\1\DATA\OCT0301\23080.D Vial: 7 Acq On 3 Oct 2001 6:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.385 142 146 154 rBV 25140 58402 1.63% 0.288% 2 6.486 154 157 168 rW 38193 107257 2.99% 0.528% 3 6.623 168 172 180 rW 19918 50152 1.40% 0.247% 4 6.733 - 180 184 198 rVB 27069 66983 1.87% 0.330% 5 713 719 728 rVB 29254 68328 1.91% 0.337%

6 11.783 728 734 752 rBV 1019802 2505870 69.96% 12.346% 7 1121 355-7-4^- 1128 1145 rBV 1588877 3423223 95.57% 16.865% 8 1697 1704 1719 rBV 1653782 3581961 100.00% 17.647% 9 25TTt2~^'^179 2186 2199 rBV 1540167 3288662 91.81% 16.202% 10 27.105>^2398 2403 2409 rBV 51756 97121 2.71% 0.478%

11 29.528 2662 2667 2675 rBV 132509 262461 ■ 7.33% 1.293% 12 29.647 2675 2680 2685 rBV 32168 60414 1.69% 0.298% 13 29.776 2690 2694 2700 rBV 24077 45924 1.28% 0.226% 14 30.722 2790 2797 2806 rBV 47462 97007 2.71% 0.478% 15 31.667 2895 2900 2905 rBV2 111750 217137 6.06% 1.070%

16 31.759 2905 2910 2916 rW 92387 182587 5.10% 0.900% 17 32.760 3013 3019 3027 rBV 86062 181734 5.07% 0.895% 18 33-;154- • 3054 3062 3078 rBV2 1210699 2888263 80.63% 14.230% 19 33.714 3115 3123 3132 rBV 98117 210986 5.89% 1.039% 20 34.632 3212 3223 3233 rBV 70551 168374 4.70% 0.830%

21 35.523 3315 3320 3327 rBV 54660 120949 3.38% 0.596% 22 36.386 3409 3414 3422 rBV 32742 78822 2.20% 0.388% 23 3502 3511 3524 rBV2 848636 2534749 70.76% 12.488%

Sum of corrected areas: 20297366

23080.D NP091101.M Tue Oct 09 10:01:12 2001

NYC-WTC_000087822

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NYC-WTC_000087822Source: NYC Law Department, mirrored locally

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