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GC/MS analysis results for sample AD22913, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22913 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087517–000087539

Folder label: “GC/MS Scan 9/20/01

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Data File : C:\HPCHEM\1\DATA\OCT0201\22913.D Vial: 3 ' • Acq On : 2 Oct 2001 4:04 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC R.T. first max last PK peak peak peak % of min scan scan scan TY height area % max. total

6.384 142 146 153 rBV 22424 53641 1.44% 0.258% >6.485 153 157 161 rBV 38458 77073 2.08% 0.371% 3 ^623 168 172 180 rVB 17712 37431 1.01% 0.180% 4 6.\33 180 184 191 rVB 26956 53136 1.43% 0.256% 5 11.6 715 719 728 rVB 28382 67510 1.82% 0.325% 6 11.782 728 734 753 rBV 1050135 2612304 70.37% 12.584% 7 1122 1128 1145 rBV 1689280 3593702 96.80% 17.311% 8 20.6fr7' 1697 1704 1721 rBV 1684965 3712436 100.00% 17.883% 9 2^ . -Hr2 2179 2186 2198 rBV2 1605198 3397191 91.51% 16.365% 10 27.104 2398 2403 2410 rVB 29122 56652 1.53% 0.273% 11 29.5377 2662 2668 2675 rBV 93071 176134 4.74% 0.848% 12 29.647 2675 2680 2686 rW 26089 48935 1.32% 0.236% 13 30.730/ 2793 2798 2804 rVB 40831 76062 2.05% 0.366% 14 31.667/2895 2900 2905 rBV2 72949 141152 3.80% 0.680% 15 31.759/ 2905 2910 2917 rW 74484 152344 4.10% 0.734% 16 32.7597 3013 3019 3025 rBV 79877 157115 4.23% 0.757% 17 »3'.154 3054 3062 3078 rBV2 1283139 3010629 81.10% 14.503% 18 33.714/ 3116 3123 3132 rBV 89468 191421 5.16% 0.922% 19 34.641> 3219 3224 3230 rVB 65016 137405 3.70% 0.662% 20 35.523/ 3316 3320 3330 rVB 58251 123648 3.33% 0.596% 36.3861/ 3409 3414 3423 rBV 21 34411 87046 2.34% 0.419% 22 -3X.^76 . 3502 3511 353 0 rBV2 945042 2796215 75.32% 13.470%

Sum of corrected areas; 20759182 22913.D NP091101.M Wed Oct 03 09:30:52 2001

NYC-WTC_000087522

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