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GC/MS calibration data for TCLP method, Oct 2001

Machine-extracted title · confidence 100%

Calibration table and chromatographic data for GC/MS analysis using the TCLP method, recorded on October 3-4, 2001.

NYC-WTC_000087722–000087730

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document direct ircicenc neporc

Data File C;\HPCHEM\1\DATA\OCT0301\LB.D Vial; 2 Acq On 3 Oct 2001 1:37 pm Operator; 209 GALOS Sample 9/21 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks; 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5

Signal ; TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.372 141 145 153 rBV 20404 47060 1.22% 0.235% 2 6.473 153 156 160 rBV 31782 64562 1.68% 0.322% 3 6.730 180 184 191 rVB 20010 44905 1.17% 0.224% 4 11.642 715 719 729 rBV 27940 68358 1.78% 0.341% 5 11.779 729 734 748 rBV 1015017 2669182 69.39% 13.314% 6 15.396 1122 1128 1142 rBV 1753191 3690271 95.93% 18.408% 7 20.684 1697 1704 1715 rBV 1811396 3846855 100.00% 19.189% 8 25.109 2179 2186 2199 rBV2 1633344 3591073 93.35% 17.913% 9 27.101 2398 2403 2409 rBV 43171 86063 2.24% 0.429% 10 33.151 3055 3062 3082 rBV2 1337133 3161595 82.19% 15.771% 11 37.273 3501 3511 3528 rBV2 958451 2777500 72.20% 13.855%

Sum of corrected areas: 20047424 LB.D NP091101.M Fri Oct 05 14:20:13 2001

NYC-WTC_000087726

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NYC-WTC_000087726Source: NYC Law Department, mirrored locally

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