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GC/MS analysis results for sample AD23082, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD23082 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087875–000087892

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\OCT0401\23082.D Vial: 2 Acq On 4 Oct 2001 4:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK' peak peak’ peak % of # min scan scan scan TY height area % max. total

1 6.374 141 145 152 rBV 17518 39602 1.08% 0.204% 2 6.475 152 156 160 rBV 27472 56239 1.53% 0.290% 3 6.723 179 183 195 rVB 18851 49045 1.33% 0.253% 4 11.643 715 719 728 rVB 26210 65846 1.79% 0.340% 5 11.781 729 734 751 rW 953273 2498423 67.86% 12.900%

6 15.398 1121 1128 1144 rBV 1633613 3478105 94.47% 17.959% 7 20.686 1697 1704 1725 rBV 1677752 3681539 100.00% 19.009%., 8 25.111 2179 2186 2198 rBV 1566746 3311827 89.96% 17.100% 9 27.103 2396 2403 2411 rBV 53926 99140 2.69% 0.512% 10 29.526 2661 2667 2672 rBV 62177 119861 3.26% 0.619%

11 30.729 2791 2798 2805 rVB 21395 41661 1.13% 0.215% 12 31.665 2895 2900 2906 rBV2 55482 104409 2.84% 0.539% 13 31.757 2906 2910 2919 rVB 40944 82840 2.25% 0.428% 14 32.758 3014 3019 3025 rBV 43183 86388 2.35% 0.446% 15 33.153 3054 3062 3076 rBV2 1220828 2841464 77.18% 14.671%

16 33.713 3112 3123 3130 rBV2 50055 108313 2.94% 0.559% 17 34.631 3219 3223 3229 rVB 35433 73502 2.00% 0.380% 18 35.521 3315 3320 3327 rBV 30743 66210 1.80% 0.342% 19 36.384 3409 3414 3421 rBV2 19387 45570 1.24% 0.235% 20 37.265 3502 3510 3530 rBV2 854224 2517383 68.38% 12.998%

Sum of corrected areas: 19367367

23082.D NP091101.M Tue Oct 09 12:23:01 2001

NYC-WTC_000087880

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NYC-WTC_000087880Source: NYC Law Department, mirrored locally

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