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GC/MS analysis results, sample AD22919, October 2001

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Gas chromatography-mass spectrometry analysis of sample AD22919 conducted on October 5, 2001, identifying other unknown compounds.

NYC-WTC_000087623–000087643

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document ijtic Area percent Report Data File C:\HPCHEM\1\DATA\OCT0201\22919.D Vial: 9 Acq On 2 Oct 2001 9:56 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCIjP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak .peak % of # min scan scan scan TY height area % max. total 1 6.375 141 145 150 rBV 20444 45922 1.42% 0.263% 2 6.476 152 156 159 rBV 32200 58819 1.82% 0.337% 3 6.614 167 171 179 rVB 16146 36390 1.13% 0.208% 4 6.724 179 183 191 rVB 23482 48453 1.50% 0.277% 5 11.645 715 719 727 rBV 24714 59990 1.86% 0.343% 6 729 734 748 rW 855123 2328976 72.14% 13.326% 7 iTTTmr 1122 1128 1144 rBV 1506609 3173456 98.30% 18.158% 8 1697 1704 1718 rBV 1510100 3228453 100.00% 18.473% 9 25-.ll» 2179 2186 2198 rBV 1367909 2897546 89.75% 16.579% 10 27.105^ 2398 2403 2410 rVB 43557 78734 2.44% 0.451% 11 29.528 2663 2667 2674 rBV 62871 123928 3.84% 0.709% 12 30.731 2793 2798 2804 rBV 20277 38880 1.20% 0.222% 13 31.667 2895 2900 2906 rBV 50300 93285 2.89% 0.534% 14 31.759 2906 2910 2916 rVB 40307 82206 2.55% 0.470% 15 32.760 3014 3019 3025 rBV 42112 81467 2.52% 0.466% 16 3055 3062 3082 rBV2 1104125 2538769 78.64% 14.526% 17 33.714 3115 3123 3130 rBV2 49195 105164 3.26% 0.602% 18 34.632 3214 3223 3231 rVB 36120 82102 2.54% 0.470% 19 35.523 3315 3320 3327 rBV 31240 67262 2.08% 0.385% 20 36.386 3409 3414 3421 rBV 18189 49441 1.53% 0.283% 21 3501 3510 3525 rBV2 769305 2257665 69.93% 12.918%

Sum of corrected areas: 17476908 22919.D NP091101.M Thu Oct 04 10:03:16 2001

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