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GC/MS analysis results for sample AD22915, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22915 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087562–000087574

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0201\22915.D Vial: 5 Acq On 2 Oct 2001 6:01 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 3 2-Pentanol, 4-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.52 ug/1 65043 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual

(1/ 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 83 2 2-Hexanol 102 C6H14O 000626-93-7 78 3 2-Butanol 74 C4H10O 000078-92-2 50 4 2-Pentanol, 3-methyl-____________ 102 C6H14O 000565-60-6 39 Abundance Scan 183 (6.725 min): 22915.D (-) m/z 44.95 100.00% 4)5

5000

69 6.40 6.60 6,80 7.00 I'''' I'''' I T ■m/z 41.05 17793% tVz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63545:2-Pentanol, 4-methyl- 4fe

5000 6.40 6.60 6.80 7.00 69 m/z 69.10 16.55% ‘' IV I I" " I " " I'' “ 27 3941 57 'I" '' " I " " I " ■n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol 4)5 ......... ............. _64g_6;60_a80_^t0__ 5000 m/z 43705 15.81%

69 19 2/31 4^ 56 tVz-> 10 I I I rrrn I I I I rrri I I I I I iTTTp i i i |-rt+l 15 20 25 30 35 40 45 50 55 60 65 . I70.... .... 75 80 85 90 95 Abundance #62568:2-Butanol ' I ' ' ' ' I 4$ 6.40 6.60 6.80 7.00 TnTz 43.95 9.30% 5000

27 59 56 72 •'I"I'I'H.I.I•.I..I.I..•IJ...,IH Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

22915.D NP091101.M Wed Oct 03 09:58:53 2001 Page 3

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NYC-WTC_000087571

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