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GC/MS analysis results for sample AD22915, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22915 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087562–000087574

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087570
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22915.D Vial: 5 Acq On : 2 Oct 2001 6:01 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params-. LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.51 ug/1 63870 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexant me 100 C6H12O 000591-78-6 87 2 Oxiraite, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 86 3 Met)ayl Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 27fiexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 39 ^bun><nce Scan 156 (6.477 min): 22915.D (-) m/z 42.95 100.00% 4)3

58 5000

71 85 100 6.20 6.40 6.60 6.80 53 1 . ....... nn"|Hiirr.... ||.II| m/z 58.05 56.13% p ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556: 2-Hexanone 43

58 5000- 6.20 6.40 6.60 6.80 m/z SYT^O 16767% 27 71 85 100 ....... . |.1h|mm| ^,,.,.,^,.,.,,1^... Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Mjundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 413 58 6.20 6.^ 6.60 6.80 5000 "mTz 41.05 14.14% 71 30 52 I 66 85 100 TtTTTTp+M +TrrrrrPTTT Ti/2-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63354: Methyl Isobutyl Ketone 4(3 6.20 6.40 6.60 6.80 m/z 99.95 9747% 5000 58 85 100 67 • ’I' " • I ’'. • I • 111111 I'' " I *''' I ' I'''' I " '' I' ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

22915.D NP091101.M Wed Oct 03 09:58:51 2001 Page 2

NYC-WTC_000087570

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NYC-WTC_000087570Source: NYC Law Department, mirrored locally

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