GC/MS analysis results for sample AD22652, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22652.D Vial: 11 Acq On : 28 Sep 2001 10:14 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method- : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 6.75 0.58 ug/1 75139 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 78 2 2-He3^ol 102 C6H14O 000626-93-7 78 3 2-H^anol, (S)- 102 C6H14O 052019-78-0 56 4 2>!Butanol 74 C4H10O 000078-92-2 45 Abundance Scan 186 (6.746 min): 22652.D (-) m/z 44.95 10^700% 40

■n^-> 5000

psslu . ... n-, I , m/z 41 L ! IJ9 rSx , ...... L 69 .n„, .... ’ I ' • I ' I ' • I • I I « ' ' I I « « I f I I I • I » I I I I 1 « I I I I I » t I I I I I I I I I I I I I » » I I I I I I I I I I I I Cl I I I I I I I l-l I I I H I I I I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 —JU. 6.40 6.60 69.00 6.80 7.00 16.78% Abundance #63547:2-Pentanol, 4-methyl- 40

AAa 5000 6.40 6.60 6.80 7.00 “m/z 41.05 16.34% 27 ?/' ? 84 87 ■n/z-> T X 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 '" 111" I" " 11 • 111 ’ > I • I" " I'" h' I “ I" " I'

‘\bundance #63584:2-Hexanol 40 6,40 6,60 6.80 7.00 5000- m/z 44.00 12.18%

69 56 8487 -rrrrtHr TrlTrkTpTTTTT T)/Z-> 10 15 ^0 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769: 2-Hexanol. (S)- I* 4)5 6.40 6.60 6.80 7.00 in/z 43.05 11.15%

5000

19 1? 3942, 69 8487 55 '' I" I ’ I' I' 11''" I ’" h' •' I " I " ‘' I " " p • ■ 1" " I' p/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.0Q

22652.D NP091101.M Wed Oct 03 11:53:08 2001 Page 4

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