GC/MS analysis results for sample AD22652, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22652.D Vial: 11 Acq On : 28 Sep 2001 10:14 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 6.63 0.42 ug/1 55187 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 3-Hex^R61 102 C6H14O 000623-37-0 83 2 1,2x4utanediol 90 C4H10O2 000584-03-2 42 3 3z<Pentanol 88 C5H12O 000584-02-1 42 4/^mylene Hydrate_______________________ .88 C5H12O 000075-85-4 38 Abundance Scan 173 (6.627 min): 22652.D (-) m/z 55.00 100.00% 5)5 50

73 5000

41 6.20 6.40 6.60 6.80 7.00 ' I''' 11 " I ’ I' I''I 1111111 ’' 11 • > 414■ I I 1 . 1 I . H69I I . II 85 11' " • I " " ( " " I " " I ■m/z 59.05 99.77% Tiyi-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63528: 3-Hexanol 5)9

5000 31 55

73 6.20 "mTz 6.40 73:00 JL 6.60 6.80 7.00 54.35% 27 45 ....... l.ll ■ I'''' I'' • 11 " ' • I' 4+4 11" '' I ‘ 84 ' I ' I " ’ ' I TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62989-. 1,2-Butanediol 31 5b

6.20 6.40 6.60 6.80 7.00 5000 “m/z 41.05 22.92% 43 27 ' I'''' I'''' r ''' I'''' I'''' I'' ‘' I' Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62943; 3-Pentanol 5)9 6.20 6.40 6.60 6.80 7.00 “mTz 43.00 19734% 31 5000

27 41

Tl/Z-> '' i'''' I' 20 25 -rp- 30 .J4^ 40 45 50 55 11'' ’' I ’ •'' I'''' I'''' r '' ’ I'''' I ’ 60 65 70 75 80 85 90 6.20 6.40 6.60 6.80 7.00

22652.D NP091101.M Wed Oct 03 11:53:05 2001 Page 3

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