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GC/MS analysis results for sample AD22913, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22913 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087517–000087539

Folder label: “GC/MS Scan 9/20/01

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' Data File : C:\HPCHEM\1\DATA\OCT0201\22913.D Vial: 3 Acq On : 2 Oct 2001 4:04 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiple: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************-************* Peak Number 8 Octadecane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.76 1.01 ug/1 152344 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octadecane 254 C18H38 000593-45-3 91 2 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 3 Triacontane 422 C30H62 000638-68-6 91 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 2910 (31.759 min): 22913.D (-) m/z 57700 107700% 5(7

85 5000

' ' I ' ' ' ' I ' 31 40 31.60 31.80 32.00 , ,, p n'. I , r I , H 11 , , ,. I . 11 I I , , . , I., I I | | ,, , I I I I, I, , I. I, I 111, , , , 111 I , I. I I, I I I I m/z 71.00 77700% n/z-> 40 60 80 100120140160180200220 240260280300320 340360380400420 Abundance #71561: Octadecane 57

5000 85 .... /v.U... 31.40 31.60 31,80 32.00 m/z 43.05 70.66% I j/1^,7^;,.............. 224 2^ |Ti.q flfiI.)I. jTii)111■1111■■I< 111111111 << <111 I > X 11 <.. I pTn 11 < 1111111111111 ■ I > 11 Ti/z-> 40 60 80 100120140160180200220240260280 300320340360380 400420 Abundance #51002: Heneicosane, 11 -(1 -ethylpropyl)- 43

71 31 40 31.60 31.80 32.00 5000 m7z 87705 49790%

■n/z-> Abundance '" I Im 183 ' I" " I" " I' I" " I 40 60 80 100120140160180200220 240260280300320 340360380400420 #55461: Triacontane 225 295 338 " I" " I"'' I''I" " I" " I" " I"'' I" " I"'' I"'

43 31.40 31.60 31.80 32.00 m/z41.0525.50% 71 5000

239 267 379 4^ pTTTJTTTTpTTTpTT-TlTT^^ pTTTpTrrpTTTpTTr|TrTTpT^^ Ti/z-> 40 60 80 100120140160180200220 240260280 300320 340360380 400420 31.40 31.60 31.80 32.00

22913.D NP091101.M Wed Oct 03 09:31:14 2001 Page 8 I

NYC-WTC_000087531

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NYC-WTC_000087531Source: NYC Law Department, mirrored locally

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