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GC/MS analysis results for sample AD22913, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22913 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087517–000087539

Folder label: “GC/MS Scan 9/20/01

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Data File : C;\HPCHEM\1\DATA\OCT0201\22913 .D Vial: 3 Acq On : 2 Oct 2001 4:04 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Octadecanoic acid, 2-methylpro Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.67 0.94 ug/1 141152 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecanoic/acid, 2-methylpropyl e 340 C22H4402; 000646-13-9 70 2 Butyl tetraraecanoate (myristate) 284 C18H36O2; 000000-00-0 64 3 Oxirane, ,3-bis(l-methylethyl)t 128 C8H16O 054644-32-5 37 4 1-Hexe^ , 5-methyl- 98 C7H14 003524-73-0 25 Abundance y Scan 2900 (31.667 min): 22913. D (-) m/z 56.00 100.00% 53

5000 4 73 ■ ■ T IL 0-7 ^29 285 , I, JJ , A, 11 , I 1^157171241 1 _3t40_3t6g_^t80_3Zpp_

n/z-> TTYTTrT7TT*l‘q‘TVrTyT~rVfYT‘T‘'T"Tp-TT-TYrT^rTph-TT-yTTTTYrTTT^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 J# m/z 57.00 50.35% Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 5)7

5000 rm 31.40 31.60 31.80 32.00 285 Wz 43.05 42.63% 267 J 111111) 11. r 1. 11.1 241 I I 1 • • • > 1 • > • ' 1 > > • • I I I > • I •! > > 1 "1 . . I 340 rr-bn TT/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate)

-rreryr-Pi-i < .Y ■ trOfTT-er-i 31.40 31.60 31.80 32.00 5000- Wz 41705 35.81% 229 211 1 '29 284 T'''' I '' ' ' I I TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 31.40 31.60 31.80 32.00 41 m/z 73.00 34.03%

5000-

73

I, l,.,l .. ................................. tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22913.D NP091101.M Wed Oct 03 09:31:11.2001 Page 7

NYC-WTC_000087530

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NYC-WTC_000087530Source: NYC Law Department, mirrored locally

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