NYC 9/11 Public Portal Document
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Data File : C;\HPCHEM\1\DATA\OCT0201\22913 .D Vial: 3
Acq On : 2 Oct 2001 4:04 pm Operator: 2 09 GTkLOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 7 Octadecanoic acid, 2-methylpro Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
31.67 0.94 ug/1 141152 Chrysene-dl2 33.15
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Octadecanoic/acid, 2-methylpropyl e 340 C22H4402; 000646-13-9 70
2 Butyl tetraraecanoate (myristate) 284 C18H36O2; 000000-00-0 64
3 Oxirane, ,3-bis(l-methylethyl)t 128 C8H16O 054644-32-5 37
4 1-Hexe^ , 5-methyl- 98 C7H14 003524-73-0 25
Abundance y Scan 2900 (31.667 min): 22913. D (-) m/z 56.00 100.00%
53
5000
4 73
■ ■ T
IL 0-7 ^29 285
, I, JJ , A, 11 , I 1^157171241 1 _3t40_3t6g_^t80_3Zpp_
n/z->
TTYTTrT7TT*l‘q‘TVrTyT~rVfYT‘T‘'T"Tp-TT-TYrT^rTph-TT-yTTTTYrTTT^
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
J# m/z 57.00 50.35%
Abundance #48214: Octadecanoic acid, 2-methylpropyl ester
5)7
5000 rm
31.40 31.60 31.80 32.00
285 Wz 43.05 42.63%
267 J
111111) 11. r 1. 11.1
241 I I
1 • • • > 1 • > • ' 1 > > • • I I I > • I •! > > 1 "1 . . I
340
rr-bn
TT/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
Abundance #40186: Butyl tetradecanoate (myristate)
-rreryr-Pi-i < .Y ■ trOfTT-er-i
31.40 31.60 31.80 32.00
5000- Wz 41705 35.81%
229
211
1 '29 284
T'''' I '' ' ' I
I
TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans-
31.40 31.60 31.80 32.00
41 m/z 73.00 34.03%
5000-
73
I, l,.,l .. .................................
tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00
22913.D NP091101.M Wed Oct 03 09:31:11.2001 Page 7
NYC-WTC_000087530
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