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GC/MS analysis results for sample AD22913, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22913 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087517–000087539

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087528
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Data File C:\HPCHEM\1\DATA\OCT0 201\22913.D Vial: 3 Acq On 2 Oct 2001 4:04 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Oxirane, 2,3-bis(1-methylethyl Concentration Rank 2 R.T. EstConc Area. Relative to ISTD R.T. 29.54 1.17 ug/1 176134 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2,3-bis(1-methylethyl) -, t 128 C8H16O 054644-32-5 32 2 1-Hex^e, 2-methyl- 98 C7H14 006094-02-6 27 3 Butyl h^adecanoate 312 C20H40O2 000000-00-0 25 4 1,3-Hexai^iol, 2-ethyl-____________ 146 C8H18O2 000094-96-2 17 Abundance \ Scan 2668 (29.537 min): 22913.D (-) Tm/z 56700 100.00% 53

5000- 4' 129 "' 29.20 29.40 29.60 29.80 312 . .... . m/z SYTOO 47.06% Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis{1-methylethyl)-, trans- 53 41

5000 '' r' 1' 11' ‘ ' f'' ’' I' I

m 29.20 29.40 29.60 29.80 m/z 43.05 77744% 113128 I' *'' I'''' r ''' I' *'' I'' ‘' I'''' I'''' I I ' ' ' ' I ’ ' ' ' I ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ^bundance

5000 41 53 #1354:1-Hexene, 2-methyl-

Ma 29.20 29.40 29.60 29.80 m/z 41.05 35.97% 27

Ti/z-> 20 1 VC 40 I 70

60 98 I ' ' ’ ’ J I ' ' ' ' I r. I I I . . 1 I I I • • . I 80 100 120 140 160 180 200 220 240 260 280 300 I' ' ' ' I

Abundance #44549: Butyl hexadecanoate . I ] TT , I I . 7 , 1 I 1 , I .1 I 5 29.20 29.40 29.60 29.80 in/z 73.00 29.38%

5000 258 1 73 240 312 129

J I I?\|l I 157171 M I ' ' ' ' I Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

22913.D NP091101.M Wed Oct 03 09:31:07 2001 Page 5

NYC-WTC_000087528

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NYC-WTC_000087528Source: NYC Law Department, mirrored locally

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