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GC/MS analysis results for sample AD22652, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087274–000087302

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report ■ Data File : C:\HPCHEM\l\DATA\SEP2801\22652.D Vial: 11 Acq On ; 28 Sep 2001 10:14 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSGINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.388 143 147 153 rBV 30763 62841 1.70% 0.280% 2 6.489 154 158 167 rW 45872 120897 3.28% 0.539% 3 6.627 170 173 182 rW 23749 55187 1.50% 0.246%

L‘6 6.746 11.648 182 715 186 720 729 735 757 196 rVB 729 rBV rW 33101 29885 1054683 75139 72241 2.04% 1.96%

2604316 70.58% 0.335% 0.322%

11.603% 7 1122 1129 1146 rBV 1672255 3572071 96.80% 15.915% 8 1697 1705 1720 rBV 1700824 3690003 100.00% 16.441% 9 2180_____ ___ 2199 2187_____ rBV2 1522688 3447157 93.42% 15.359% 10 29.5411/ 2663 2669 2674 rBV 122630 233598 6.33% 1.041% 11 29.651 J 2677 2681 2687 rVB 34078 69545 1.88% 0.310% 12 29.789 2689 2696 2702 rVB 20664 43297 1.17% 0.193% 13 30.734 2794 2799 2806 rBV 54453 109916 2.98% 0.490% 14 .31.680 2897 2902 2907 rBV 96818 192015 5.20% 0.856% 15 31.772 y 2907 2912 2918 rVB 111757 213506 5.79% 0.951% 16 32.763-^ 3015 3020 '3025 rBV 115619 225393 6.11% 1.004% 17^^33-,-X6;i 3056 3064 3076 rBV2 1283633 3057521 82.86% 13.623% 18 33.718/3117 3124 3135 rVB 128402 276569 7.50% l.'232% 19 34.645:4 3220 3225 3230 rVB 105325 203629 5.52% 0.907% 20 35.535/ 3317 3322 3331 rBV 87459 194508 5.27% 0.867% 21 36.398/ 34nr3416 3428 rVB 56239 129259 3.50% 0.576% 22 37.289 3504 3513 3533 rBV2 929567 2866606 77.69% 12.772% 23 38.179 >' 3604 3610 3619 rVB3 18289 67537 1.83% 0.301% 24 38.418 y3632 3636 3644 rVB2 18608 50511 1.37% 0.225% 25 39.786/ 3778 3785 3799 rVB 42751 210973 5.72% 0.940% 41.787 73993 4003 4024 rVB3 26 49232 319969 8.67% 1.426% 27 44.266 J 4267 4273 4291 rVB4 41090 280142 7.59% 1.248%

Sum of corrected areas: 22444346 22652.D NP091101.M Wed Oct 03 11:52:54 2001

NYC-WTC_000087279

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