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GC/MS analysis results for sample AD22652, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087274–000087302

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22652.D Vial; 11 Acq On : 28 Sep 2001 10:14 pm Operator; 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Nonadecane, 9-methyl- Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 29.65 0.45 ug/1 69545 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual f lyNonadecane, 9-methyl- 282 C20H42 013287-24-6 91 ^2 Dodecane, 1-iodo- 296 C12H25I 004292-19-7 86 3 Eicosane, 10-methyl- 296 C21H44 054833-23-7 86 4 Hexadecane 226 C16H34 000544-76-3 86 Abundance Scan 2681 (29.651 min): 22652.D (-) m/z 57.00 100.00% 5/

71 43 5000 85

99 29.40 29.60 29.80 30.00 207 It I'''' I'''' I m/z 71.10 66783% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #39865: Nonadecane, 9-methyl- 5|7

71 85 5000 29.40 29.60 29,80 30.00 99 140 m/z 43.00 60731% 168 1 ,I , J 252 282 Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #41998: Dodecane. 1-iodo- 57 71 T 29.40 29.60 29.80 30.00 43 85 m/z 85.05 45.31% 5000

^113127,4,^5^169.................................................... I I I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 43 #42197: Eicosane, 10-methyl- /YA... . 29.40 29.60 29.80 30.00 m/z 41.00 28761% 71 5000 85

99 I IIS ..X 154.168 H 1 'I‘ I, ,1 141 II ji ................ 2^^ 296 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.40 29.60 29.80 30.00

22652.D NP091101.M Wed Oct 03 11:53:15 2001 Page 7

NYC-WTC_000087287

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NYC-WTC_000087287Source: NYC Law Department, mirrored locally

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