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GC/MS analysis results for sample AD22652, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087274–000087302

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22652.D Vial: 11 Acq On : 28 Sep 2001 10:14 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclobutane, 1,2-diethyl-, tra Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

29.54 1.53 ug/1 233598 Chrysene-dl2 33.17

Hit# of 5 mtative ID MW MolForm CAS# Qual

1 Cyclobu e, 1,2-diethyl-, trans- 112 C8H16 019341-98-1 27 2 l-Hexehe, 2-methyl- 98 C7H14 006094-02-6 27 3 Butyz hexadecanoate 312 C20H40O2 000000-00-0 25 4 1,3 Hexanediol, 2-ethyl-__________ 146 C8H18O2 000094-96-2 25 Abundance Scan 2669 (29.541 min): 22652.D (-) m/z 56.00 100.00% 3

5000 4 73 257 -I 1-)-, T|-T-| ^29 239 29.20 29.40 29.60 29.80 312 I'-'.. . m/z SYTOO 45773% Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #2701: Cyclobutane, 1,2-diethyl-, trans- 4)1 53

5000 27 29.20 29.40 29.60 29.80 70 84 m/z 43.05 36.71% . J 112 11 I if I I I I I p I I I j I • . I I I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Sibundance #1354:1-Hexene. 2-methyl- 53 T 41 29.20 29.40 29.60 29,80 5000 m/z 41.05 35.15% 27 -X... 98 ■p-m-yr-m-f iVz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 5b 29.20 29.40 29.60 29.80 m/z 73.00 31.38%

5000 258 J 73 240 312 129

-n/z-> 20 40 1 80 100 120 140 160 180 200 220 240 260 280 300 60 f ’ I I I . i > I I I I I M I I I I I I I I I I I 2920 29.40 29.60 29.80

22652.D NP091101.M Wed Oct 03 11:53:12 2001 Page 6

NYC-WTC_000087286

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