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GC/MS analysis results for sample AD22558, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22558 conducted on October 1, 2001, identifying unknown compounds.

NYC-WTC_000087097–000087119

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087107
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2701\22558.D Vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator: GALOS ■ Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 10.39 0.63 ng/uL 95874 1,4-Dichlorob'enzene-d4 11.97 Hit# 5 Tentative ID MW MolForm CAS# Qual

1 3yHexanol 102 C6H14O 000623-37-0 42 2 Vnexanol 102 C6H14O 000623-37-0 40 3 /-Hexanol 102 C6H14O 000623-37-0 40 4/3-Hexanol 102 C6H14O 000623-37-0 40 [Abundance Scan 606 (10.392 min); 22558.D (-) m/z 59 716 100.00% 43 5b

5000 73 M 85 10 00 10.20 10.40 10.60 10.80 I''' ‘ I " '' I' " ' I'' " I'''' I .. ..... Ill'l m/z 43710 90778% ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762; 3-Hexanol $

31 5000 ...................... 43 73 10.00 10.20 10.40 10.60 10.80 m/z 55716 79723% 44 102 " I" " I' - n+ I" ’ 'T r Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ^bundance #63527; 3-Hexanol 5)9 A 10 00 10.20 10.40 10.60 10.80 c 253 73 m/z 73765 43.13% 31

45 84 4- 4# n I'"' I''" I"'' I n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ^bundance #63529; 3-Hexanol 1I T 5)9 10.00 10.20 10,40 10.60 10.80 m/z41710 42.53% 31 5000 73

44 I I I I I I p-l I ■ I I I I ■ I I I ■ I I I I ■ I I I I I I I I I I I 4 I I I I I I I I I I I I I I I I I I I I I I I I I I I I |H I I I I I I , p I I I IIIIIII , I,,,,,,,, \, A,,, Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 10.00 10.20 10.40 10.60 10.80

22558.D NP072501.M Mon Oct 01 14:52:16 2001 Page 3

NYC-WTC_0000'87107

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NYC-WTC_000087107Source: NYC Law Department, mirrored locally

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