Calibration data table for TCLP analysis including retention times and response factors for various compounds.
NYC-WTC_000086981–000087006Folder label: “508 Scan 9/17/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCTO101\LBD.D Vial: 4 Acq On 1 Oct 2001 4:39 pm Operator:- 20 9 GALOS • Sample 9/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ************ * * ******************************************************* Peak Number 2 2-Hexanone Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.97 ug/1 129681 1,4-Dichlorobenzene-d4 11.79 Hit# of >5 Tentative ID MW MolForm CAS# Qual 1 2-He: none 100 C6H12O 000591-78-6 91 2 Oxir .ne, 2-methyl-2-(1-methylethyl) 100C6H12O 072221-03-5 80 3 Methlyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 27Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 Abundance Scan 158 (6.492 min): LBD.D (-) Wz 42.95 100.00% 4)3
58 5000
51 I 71 85 100 6.20 6.40 6.60 6.80
■n/z-> Ah 1 " I I I I I I I I I r I I I I I I I I I I I I I I I I I I I I I I ) I I I I I I H I I I I I I I I I I I I
20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 p m/z 58.00 58.74% Abundance #1556:2-Hexanone 43
58 5000 ' ' 6.20' 6.40 6.60 6.80 m/z :41.05 16.78% 27 71 85 100 111 ■,, 11.. I.." 111. ■ 11... 11.,, I," 11
nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 4)3 58 ' ' I ' ' ' ' I ' ' ' ' I ’ ' ' 6.80 6.20 6.40 6.60 5000 m/z 57.00 16.61% 71
30 66 85 . 100 4- ........'I'' i'''' I'''' I'''' I'''' I ‘' I'''' I' Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63351: Methyl Isobutyl Ketone 4)3 6.20 6.40 6.60 6.80 m/z 100.05 9.86%
Jl 552 58 27 85 100 TTJT Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80
LBD.D NP091101.M Tue Oct 02 12:28:09 2001 Page 2
NYC-WTC_000086988
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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