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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample 9/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 6.39 0.49 ug/1 65890 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual 1 3-» :anone 100 C6H12O 000589-38-8 90 2 3- ;ntanone, 2-methyl- 100 C6H12O 000565-69-5 47 3 B ane, 2,2-dimethyl- 86 C6H14 000075-83-2 45 4 Furanmethanamine, tetrahydro- 101 C5H11NO 004795-29-3 38 ZKbundance Scan 147 (6.391 min): LBD.D (-) m/z 43.00 100.00% 43 57

71 5000 100

6.00 6.20 6.40 6.60 6.80 l|'^P'>'l' *.. . +rrrT r m/z 57700 90.99% m/z-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #63358: 3-Hexanone I 57

c 71 253 6.00 6.20 6.40 6.60 6.80 100 m/z 71.00 57.76%

m/z-> J + ++TTT,-rjTTTTT ...................... 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 P Abundance #63398:3-Pentanone, 2-methyl- 5(7 43 . I . . 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 34.64%

I k 100 71

85 I" "I ......... . ..... . t-,Ty P " I' " ' I'"' I m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #732: Butane, 2,2-dimethyl- 43 5|7 6.00 6.20 6.40 6.60 6.80 71 ■niTz 41.05 24.17% 29 5000

15 +PTTtpt+tt .... I iTTJTTTTpTrrfTTrrpTTT^^ pi/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

LBD.D NP091101.M Tue Oct 02 12:28:05 2001 Page 1

NYC-WTC_000086987

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NYC-WTC_000086987Source: NYC Law Department, mirrored locally

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GC/MS calibration table, Oct 1 2001 · Box DEP Box 67

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