Calibration data table for TCLP analysis including retention times and response factors for various compounds.
NYC-WTC_000086981–000087006Folder label: “508 Scan 9/17/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On : 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample : 9/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 18
R.T. EstConc Area Relative to ISTD R.T.
6.63 0.48 ug/1 64780 1,4-Dichlorobenzene-d4 11.79
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Hexan61 102 C6H14O 000623-37-0 74 2 AmyleXe Hydrate 88 C5H12O 000075-85-4 40 3 Sil^e, trimethyl- 74 C3H10Si 000993-07-7 36 4 3-pentanol 88 C5H12O 000584-02-1 33 Abundar^/e Scan 173 (6.630 min): LBD.D (-) m/z 59.05 100.00% I 73 5000 43 6.20 6.40 6.60 6.80 7.00 53 84 ' ''i ' ' ' I ' ‘ ‘ ' i ' ‘ ' I ' ' ' ‘ I “m/z 55.00 68.97% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63529: 3-Hexanol 5(9
5000- 31 73 ' I ' ' ' ' I ' ' ~ 6.20 6.40 6.60 6.80 7.00 m/z 73.00 51.00% 44 —I—r—I—I—|—I—r-rA—l-^ 4H- 102 -T-+ mZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #849; Amylene Hydrate 5(9 ............... f....... 6.20 6.40 6.60 6.80 7.00 5000 73 m/z 43.00 26.51% 31
' I ‘' I'' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62564: Silane, trimethyl- 5b 6.20 6.40 6.60 6.80 7.00 "m/z 417705 25.99%
5000- 73
15 31 45 I m/z~> 10 20 30 40 50 60 70 80 90 100 110 6.20 6 40 6.60 6.80 7,00
LBD.D NP091101.M Tue Oct 02 12:28:12 2001 Page 3
NYC-WTC_000086989
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NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Laboratory results for sample AD22542 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22543 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22544 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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