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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On 1 Oct 2001 4:39 pm Operator: 209 ■ GALOS Sample 9/17 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.391 142 147 154 rBV 29871 65890 1.74% 0.271% 2 6.492 154 158 168 rW 47562 129681 3.43% 0.534% 3 6.630 169 173 182 rW 25013 64780 1.71% 0.267% 4 6.740 182 185 202 rVB 33325 86262 2.28% 0.355% 5 7.768 293 297 308 rBV 56318 132999 3.51% 0.548% 6 11.643 715 719 729 rBV 29315 67616 1.79% 0.279% 7 11.789 729 735 749 rBV 1052935 2674361 70.67% 11.019% 8 15.397 1122 1128 1145 rBV 1649519 3662586 96.78% 15.090% 9 20.685 1697 1704 1719 rBV 1696357 3784397 100.00% 15.592% 10 25.119 2180 2187 2198 rBV 1590192 3489129 92.20% 14.375% 11 29.535 2663 2668 2675 rBV 319469 630583 16.66% 2.598% 12 29.654 2676 2681 2689 rVB 72221 139452 3.68% 0.575% 13 29.783 2689 2695 2704 rBV2 44286 90531 2.39% 0.373% 14 30.738 2793 2799 2807 rBV 112142 231479 6.12% 0.954% 15 31.674 2896 2901 2906 rBV 235924 461621 12.20% 1.902% 16 31.766 2906 2911 2919 rW 214345 421315 11.13% 1.736% 17 32.766 3014 3020 3026 rBV 210673 440499 11.64% 1.815% 18 33.161 3055 3063 3080 rBV2 1307596 3116866 82.36% 12.842% 19 33.721 3112 3124 3131 rBV 243027 526321 13.91% 2.168% 20 34.639 3215 3224 3231 rBV 189420 408698 10.80% 1.684% 21 35.530 3316 3321 3330 rBV 167066 356038 9.41% 1.467% 22 36.393 3410 3415 3421 rBV 97681 221171 5.84% 0.911% 23 37.283 3503 3512 3527 rBV2 934039 2927805 77.37% 12.063% 24 38.412 3630 3635 3641 rBV2 25628 74233 1.96% 0.306% 25 39.670 3765 3772 3782 rBV5 17911 67214 1.78% 0.277%

Sum of corrected areas: 24271527 LBD.D NP091101.M Tue Oct 02 12:27:54 2001

NYC-WTC_000086985

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