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ICP-MS analysis report, Dec 26, 2001

Machine-extracted title · confidence 95%

Laboratory summary report detailing concentrations of Beryllium, Scandium, Vanadium, Manganese, and Indium tested December 26, 2001.

NYC-WTC_000085045–000085068

Folder label: “NEWE 12/26/01 29286 - 31380

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NYC 9/11 Public Portal Document

Method 200.8 - Summary Report Sample ID: QCS Sample Date/Time: Wednesday, December 26, 2001 10:37:56 Sample Type: Sample Description: 50 PPB Number of Replicates: 3 Batch ID: Method File: d:\elandata\Method\NEWE200.8.mth Dataset File: d:\elandata\07-18-01 to 01-03-2002\daily performance\QCS.1376 Sample Prep Volume (mL): Initial Sample Quantity (mg): Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 28720.583 0.248 0.040 50.06933 2.00 ug/L |> Sc-1 45 715826.414 1.890 715826.414 ug/L I V 51 763914.203 2.618 1.066 50.31003 3.55 mg/L L Mn 55 1041294.357 0.724 1.455 50.61271 2.61 ug/L r> In 115 1603839.564 0.246 1603839.564 ug/L I Sb 121 522824.311 0.709 0.326 50.52043 0.81 ug/L L Sb 123 402041.108 0.462 0.251 50.29357 0.24 ug/L r> Ho 165 2139555.802 1.203 2139555.802 ug/L L Tl 205 1706246.433 0.297 0.797 50.36957 1.09 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery I nt Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff r Be 9 |> Sc-1 45 97.745 I V 51 L Mn 55 r> In 115 96.319 I Sb 121 L Sb 123 r> Ho 165 100.928 L Tl 205 Calibration Analyte MassCurve Type Correlation Coefficient r Be 9Linear Thru Zero 0.999967 |> Sc-1 45Linear Thru Zero I V 51 Linear Thru Zero 0.999983 L Mn 55Linear Thru Zero 0.999997 r>' In 115 Li near Thru Zero I Sb 121 Linear Thru Zero 0.999986 L Sb 123Linear Thru Zero 0.999994 r> Ho 165Linear Thru Zero

Sample ID: QCS Report Date/Time: Wednesday, January 16, 2002 14:07:38 Page 1

NYC-WTC_000085057

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NYC-WTC_000085057Source: NYC Law Department, mirrored locally

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