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Method 200.8 ICP-MS lab results, NEWE samples, Jan 11, 2002

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ICP-MS analysis of water samples using Method 200.8 with elemental measurements (Be, Sc, Mn, In, Sb, Ho) and quality control replicates performed on January 11, 2002.

NYC-WTC_000085478–000085537

Folder label: “NEWE 1/11/2002 AD 31456 - AE00110 Batches 16390 16391 16402 copies made

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NYC 9/11 Public Portal Document

Method 200.8 - Summary Report Sample ID: AD31456 Sample Date/Time: Friday, January 11, 2002 12:55:49 Sample Type: QC Duplicate Sample Description: Number of Replicates: 3 Batch ID: Method File: d:\elandata\Method\NEWE200.8.mth Dataset File: d:\elandata\Dataset\daily performance\AD31456.2026 Sample Prep Volume (mL): Initial Sample Quantity (mg): Aliquot Volume (mL): 5e+001 Diluted To Volume (mL): 1e+002

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 13.000 7.692 0.000 0.00610 44.31 ug/L |> Sc-1 45 641069.108 2.537 641069.108 ug/L L Mn 55 867469.024 3.467 1.352 93.76459 2.98 ug/L r> In 115 1326488.544 1.654 1326488.544 ug/L I Sb 121 390.012 3.353 0.000 0.08294 3.51 ug/L L Sb 123 310.973 3.685 0.000 0.08666 2.26 ug/L r> Ho 165 1816750.613 1.696 1816750.613 ug/L L Tl 205 278.674 5.229 0.000 0.00424 26.89 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery I nt Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff r Be 9 551.674 |> Sc-1 45 100.965 L Mn 55 tZ8.933 r> In 115 100.585 I Sb 121 4.433 L Sb 123 7.771 r> Ho 165 101.153 L Tl 205 15.071 Calibration Analyte MassCurve Type Correlation Coefficient [■ Be 9Linear Thru Zero 0.999992 |> Sc-1 45Linear Thru Zero L Mn 55Linear Thru Zero 0.999983 r> In 115Linear Thru Zero I Sb 121 Linear Thru Zero 0.999998 L Sb 123Linear Thru Zero 1.000000 r> Ho 165Linear Thru Zero L Tl 205Linear Thru Zero 0.999977

Sample ID: AD31456 Report Date/Time: Friday, January 11, 2002 12:56:21 Page 1

NYC-WTC_000085491

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