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Method 200.8 ICP-MS lab results, NEWE samples, Jan 11, 2002

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ICP-MS analysis of water samples using Method 200.8 with elemental measurements (Be, Sc, Mn, In, Sb, Ho) and quality control replicates performed on January 11, 2002.

NYC-WTC_000085478–000085537

Folder label: “NEWE 1/11/2002 AD 31456 - AE00110 Batches 16390 16391 16402 copies made”

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Method 200.8 - Summary Report Sample ID: QCS 50 PPB Sample DateZTime: Friday, January 11,2002 12:46:42 Sample Type: Sample Sample Description: Number of Replicates: 3 Batch ID: Method File: d:\elandata\Method\NEWE200.8.mth Dataset File: d:\elandata\Dataset\daily performance\QCS 50 PPB.2022 Sample Prep Volume (mL): Initial Sample Quantity (mg): Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 24993.562 0.956 0.039 49.84527 1.78 ug/L Sc-1 45 633931.052 2.427 633931.052 ug/L L Mn 55 912005.018 2.410 1.438 49.86739 3.96 ug/L r> In 115 1322601.056 0.379 1322601.056 ug/L I Sb 121 437663.670 0.856 0.331 51.34776 0.49 ug/L L Sb 123 335725.092 2.369 0.254 51.32553 2.03 ug/L r> Ho 165 1795447.295 3.374 1795447.295 ug/L L Tl 205 1408723.964 4.261 0.784 50.71003 2.47 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery I nt Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff r Be 9 |> Sc-1 45 99.841 L Mn 55 r> In 115 100.290 I Sb 121 L Sb 123 r> Ho 165 99.967 L Tl 205 Calibration Analyte MassCurve Type Correlation Coefficient r Be 9Linear Thru Zero 0.999992 |> Sc-1 45Linear Thru Zero L Mn 55Linear Thru Zero 0.999983 r> In IISLinear Thru Zero 1 Sb 121 Linear Thru Zero 0.999998 L Sb 123Linear Thru Zero 1.000000 r> Ho 165 Linear Thru Zero L Tl 205Linear Thru Zero 0.999977

Sample ID: QCS 50 PPB Report Date/Time: Friday, January 11,2002 12:47:15 Page 1

NYC-WTC_000085487

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