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Method 200.8 ICP-MS lab results, NEWE samples, Jan 11, 2002

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ICP-MS analysis of water samples using Method 200.8 with elemental measurements (Be, Sc, Mn, In, Sb, Ho) and quality control replicates performed on January 11, 2002.

NYC-WTC_000085478–000085537

Folder label: “NEWE 1/11/2002 AD 31456 - AE00110 Batches 16390 16391 16402 copies made”

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Method 200.8 - Summary Report Sample ID: ICV STD2 60 PPB Sample Date/Time: Friday, January 11, 2002 12:44:34 Sample Type: Sample Sample Description: Number of Replicates: 3 Batch ID: Method File: d:\elandata\Method\NEWE200.8.mth Dataset File: d:\elandata\Dataset\daily perform a nce\ICV STD2 60 PPB.2021 Sample Prep Volume (mL): Initial Sample Quantity (mg): Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 29011.574 4.643 0.046 58.29368 3.90 ug/L |> Sc-1 45 629087.683 2.602 629087.683 ug/L L Mn 55 1058967.550 2.266 1.683 58.33427 1.94 ug/L r> In 115 1309371.244 1.029 1309371.244 ug/L I Sb 121 500269.411 1.078 0.382 59.29144 1.50 ug/L L Sb 123 388564.474 1.277 0.297 60.01432 2.04 ug/L r> Ho 165 1770388.046 1.027 1770388.046 ug/L L Tl 205 1632140.770 3.756 0.922 59.58820 3.74 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery I nt Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff r Be 9 i> Sc-1 45 99.078 L Mn 55 r> In 115 99.287 I Sb 121 L Sb 123 r> Ho 165 98.572 L Tl 205 1/ Calibration Analyte MassCurve Type Correlation Coefficient r Be 9Linear Thru Zero 0.999992 |> Sc-1 45Linear Thru Zero L Mn 55Linear Thru Zero 0.999983 r> In 115Linear Thru Zero I Sb 121 Linear Thru Zero 0.999998 L Sb 123Linear Thru Zero 1.000000 r> Ho 165Linear Thru Zero L Tl 205Linear Thru Zero 0.999977

Sample ID: ICV STD2 60 PPB Report Date/Time: Friday, January 11,2002 12:45:06 Page 1

NYC-WTC_000085486

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