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Method 200.8 ICP-MS lab results, NEWE samples, Jan 11, 2002

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ICP-MS analysis of water samples using Method 200.8 with elemental measurements (Be, Sc, Mn, In, Sb, Ho) and quality control replicates performed on January 11, 2002.

NYC-WTC_000085478–000085537

Folder label: “NEWE 1/11/2002 AD 31456 - AE00110 Batches 16390 16391 16402 copies made”

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Method 200.8 - Summary Report Sample ID: LFB 50 PPB Sample Date/Time: Friday, January 11, 2002 12:48:45 Sample Type: Sample Sample Description: Number of Replicates: 3 Batch ID: Method File: d:\elandata\Method\NEWE200.8.mth Dataset File: d:\elandata\Dataset\daily performanceMFB 50 PPB.2023 Sample Prep Volume (mL): Initial Sample Quantity (mg): Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 45 24149.954 631658.292 2.363 1.682 0.038 631658.292 48.33262 3.03 ug/L ug/L I: Se-I L Mn 55 887138.513 2.066 1.404 48.65866 1.87 ug/L n In Sb 115 121 1291137.928 417638.140 0.843 1.011 1291137.928 0.323 50.19610 1.51 ug/L ug/L L Sb 123 325186.052 0.814 0.252 50.92871 0.59 ug/L n Ho 165 1759072.604 1.840 1759072.604 ug/L L Tl 205 1356864.518 1.839 0.771 49.85534 0.86 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery I nt Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff r Be 9 |> Sc-1 45 99.483 L Mn 55 r> In 115 97.904 I Sb 121 L Sb 123 r> Ho 165 97.942 / L Tl 205 Calibration Analyte MassCurve Type Correlation Coefficient f Be 9Linear Thru Zero 0.999992 1> Sc-1 45Linear Thru Zero L Mn 55Linear Thru Zero 0.999983 r> In 11 SLinear Thru Zero I Sb 121 Linear Thru Zero 0.999998 L Sb 123Linear Thru Zero 1.000000 r> Ho 165Linear Thru Zero L Tl 205Linear Thru Zero 0.999977

Sample ID: LFB 50 PPB Report Date/Time: Friday, January 11, 2002 12:49:18 Page 1

NYC-WTC_000085488

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