VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02may23\12155.D Vial: 3 Acq On 23 May 2002 5:41 pm Operator: 201-wb Sample nys Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 2 Arsenous acid, tris(trimethyls Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.95 0.05 ug/L 38360 1,4-DIFLUOROBENZENE 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 9 2 Acetamide, N-[4-(trimethylsilyl)phe 207 CllH17NOSi 017983-71-0 7 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 IH-Indole, 5-methy1-2-phenyl-_________ 207 C15H13N . 013228-36-9 5 Abundance Scan 821 (17.945 min): 12155.D (-) m/z 207.15 100.00% “ 207

532

17.60 17.80 18.00 18.20 44 m/z 208.05 21.71% n/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #48300: Arsenous acid, tris(trimethylsilyl) ester 207

5000 "T 17.60 17.80 18.00 18.20 m/z 96.10 20.20% 73 105 133 44 h r|V..1 . . I . .7'.I, J 191 223239 327 4+rr rfVy '''' I • I " •«I " • • I" ‘ ‘ 1" " I I' ' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #24586: Acetamide, N-[4-(trimethylsiiyi)phenyl]- 207

17.60 17.80 18.00 18.20 Wlili] m/z 209.15 14.04% 150

45 73 106 . I..,.......t.... ... ..... ....I,...... .. ....... 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 17.60 17.80 18.00 18.20 m/z 44.00 3.55%

5000 179 77

T I n " I • " • I " * • I " > J1 tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 17.60 17.80 18.00 18.20

12155.D HP051702.M Thu May 23 18:20:48 2002 Page 2

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