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Volatile organic compounds blank results, Mar 1 2002

Machine-extracted title · confidence 95%

Laboratory analysis results for volatile organic compounds blank sample AE04037 dated March 1, 2002.

NYC-WTC_000020751–000020867

Folder label: “524 3/1/02 - 3/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAR01\04037.D Vial: 17 Acq On : 1 Mar 2002 11:46 pm Operator: Sample : nyc Inst : 210 Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Pyrido(2,3-d]pyrimidine, 4-phe Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

19.18 0.02 ug/L 6076 1,4-DIFLUOROBENZENE 15.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 2 Acetamide, N-[4-(trimethylsilyl)phe 207 C11H17NOS1 017983-71-0 3 3 Vanadium, (.eta.7-cycloheptatrienyl 207 C12H12V 012636-68-9 3 4 2-(1-Piperidino)-5-nitropyridine 207 C10H13N3O2 026820-61-1 2 Abundance scan 1400 (19.179 min): 04037.D (-) m/z 206.95 100.00% 207 8000 6000 4000 96 2000 133 18,80 19.00 19.20 19.40 19.60 78 ...... 44............................ .......................1................................. .-I,,.. m/z 207.95 30.51% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 8000 6000 4000 179 18,80 19.00 19.20 19.40 19.60 77 m/Z 95.95 25.27% 2000 - 103 1R2

m/z—> 30 ........... ...... T... 126....172........ ....... 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #24586: Acetamide, N-[4-(trimethylsily)pheny!]- 192 207 8000 6000 18,80 19.00 19.20 19.40 19.60 m/z 132.95 17.88% 4000 150 2000 ... 45...... 73... . ............... . ............. ।..... m/z—> 3040‘5060"70‘8090‘ 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #24588: vanadium, (.eta.7-cycloheptatrienyliumX.eta.5-2,4- 207 18,80 19.00 19.20 19.40 19.60 8000 m/z 78.05 5.91% 129 6000 51 116 4000 2000 90 39... 65.7.. |....... ' 140.... .... 181_ m/z—> 36' 4'6' ’ 5I0 ‘ 6b' 76 80'' 90' 16b' 110 120 130 140 lid 160 iro 180 190 200 210 18.80 19.00 19.20 19.40 19.60

04037.D HP021102.M Mon Mar 04 14:19:47 2002 Page 4

NYC-WTC_000020777

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NYC-WTC_000020777Source: NYC Law Department, mirrored locally

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