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VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02

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Scanned page image, NYC-WTC_000003278
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : .C:\HPCHEM\1\DATA\02JAN22\00916.D Vial: 11 Acq On : 22 Jan 2002 5:46 pm Operator: Sample : nyc Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 3 Arsenous acid, tris(trimethyls Concentration Rank 1

R.T. EstConc Area Relative to I.STD R.T. --------------------------------------------------------------------- 21.10 0.13 ug/L 40054 1,4-DIFLUOROBENZENE 17.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 59 2 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 56 3 Benzenamine, 4-bromo-2-chloro- 205 C6H5BrClN 038762-41-3 9 4 2-Methyl-7-phenvlindole 207 C15H13N 000000-00-0 7 dance Scan 1559 (21.105 min): 00916.D (-) m/ Z 206.95 100 . D 0 27

5000

96 40 133 191 20.80 21.00 21.20 21.40 75 1 i m Z 28.00% > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 dance #48300: Arsenous acid, tris(trimethyisilyl) ester 27

5000

73 105 133 44 1 147 191 i 223 239 327 •> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 idance #70586: Cyclotrisiloxane, hexamethyl- 2 7

20.80 21.00 21.20 21.40 5000 m Z 208.95 16.52r6

96 191 75 119133147 163177 > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 dance #24007: Benzenamine, 4-bromo-2-chloro- 27 20.80 21.00 21.20 21.40 m/z 40.05 11.77

5000 63 90 126

46 03 177 > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 20.80 21.00 21.20 21.40

00916.D HP010802.M Wed Jan 23 09:39:51 2002 Page 3

NYC-WTC 000003278

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NYC-WTC_000003278Source: NYC Law Department, mirrored locally

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