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VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02

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Scanned page image, NYC-WTC_000003291
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02JAN22\00918.D Vial: 13 Acq On : 22 Jan 2002 7:22 pm Operator: Sample : nyc Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Arsenous acid, tris(trimethyls Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 21.12 0.11 ug/L 33791 1,4-DIFLUOROBENZENE 17.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 72 2 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 56 3 1H-Indole, 5-methyl-2-phenyl- 207 C15H13N 013228-36-9 36 4 1H-Indole. 1-methvl-2-nhenvl- 207 C15H13N 003558-24-5 9 Scan 1560 (21.116 min): 00918.D (-) m z 206.95 100. 0Uo 27

50001

96 133 191 0.80 21.00 21.20 21.40 40 59 m z 20b.05 21.39 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 #48300: Arsenous acid, tris(trimethylsilyl) ester 27

5000 0.80 21.00 21.20 21.40 m z 96.05 14.31% 73 105 133 191 44 Ii 223239 327 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 #27918: Cyclotrislioxane, hexamethyl- 27

0.80 21.00 21.20 21.40 5000 m z 132.95 9.73%

96 191 133 15 73 115 163 222 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 #24654:1H-IndoIe, 5-methyl-2-phenyl- 2 7 0.80 21.00 21.20 21.40 m z 209.05 9.50%

5000

104 128 178 152 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 20.80 21.00 21.20 21.40

00918.D HP010802.M Wed Jan 23 09:44:10 2002 Page 4

NYC-WTC 000003291

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NYC-WTC_000003291Source: NYC Law Department, mirrored locally

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