Calibration standard analysis results, sample C5, May 2002

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Results for calibration standards including deuterated compounds analyzed on May 6, 2002.

NYC-WTC_000082506–000082517

Folder label: “525 X 4/30/02 A 5/1/02”

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Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050102\C05A0501.D Vial: 5 Acq On 1 May 2002 3:16 pm Operator: Bohlk / Inst 213 Sample CO. 5 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 06 13:01:46 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon May 06 12:42:26 2002 Response via : Initial Calibration DataAcq Meth : 050102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 17.59 164 3185690 5.00 ug/L 0.00 9) Phenanthrene d-10 21.89 188 4574810 5.00 ug/L 0.00 19) Chrysene d-12 29.62 240 3198259 5.00 ug/L 0.00 25) p-Terphenyl d-14 26.77 244 2656671m 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.55 134 757268 5.20 ug/L 0.00 Spiked Amount 5.000 Recovery = 104.00% 20) Triphenyl Phosphate 28.94 326 582641 4.09 ug/L 0.00 21) Perylene D-12 33.60 264 1956945 4.40 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.00% 26) Acenaphthene d-10 (surr) 17.59 164 3185690 4.82 ug/L 0.00 Spiked Amount 5.000 Recovery = 96.40% 27) Phenanthrene d-10 (surr) 21.89 188 4574810 5.08 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.60% 28) Chrysene d-12 (surr) 29.62 240 3198259 5.34 ug/L 0.00 Spiked Amount 5..000 Recovery = 106.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.11 237 15503 1.10 ug/L # 75 4) Hexachlorobenzene 20.76 284 103764m 0.52 ug/L 5) EPTC 15.60 128 100676m 0.47 ug/L 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 18.49 126 159064m 0.52 ug/L 10) Simazine 21.32 201 8887 0.98 ug/L # 66 11) Atrazine 21.46 200 47525m 0.65 ug/L 12) Alachlor 23.29 160 62654 0.30 ug/L 89 13) Terbacil 0.00 117 0 N.D. d 14) Acetochlor 23.08 146 33815 0.51 ug/L 98 15) Metribuzin 23.11 198 12095 0.91 ug/L , 66 16) Metolachlor 24.21 162 148226 0.24 ug/L"’^ 99 17) Butachlor 26.04 160 35380 0.73 ug/L # 59 18) 4,4'-DDE 26.66 246 80192 _0_^2 ug/L 92 22) Bis (2-Ethylhexyl) adipate 28.89 129 63331m 1.6^ug/L 23) Bis (2-Ethylhexyl) phthala 30.30 149 80751m 24) Benzo (a) pyrene 33.44 252 53553m 0.84 ug/LV‘V'

(#) = qualifier out of range (m) = manual integration C05A0501.D 050102.M Mon May 06 13:06:21 2002 Page 1

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Method 525.2 compound analysis results, May 2002 · Box DEP Box 65

NYC-WTC_000082495

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