Volatile organic compound analysis results, sample AE08425, April 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02apr08\0408C10A.D Vial: 2 Acq On 8 Apr 2002 7:11 pm Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 8 19:50 2002 Quant Results File: HP031802.RES

Quant Method C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Last Update Mon Apr 08 12:07:27 2002 Response via Initial Calibration DataAcq Meth HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.05 114 1373760 5.00 ug/L 0.00 24) CHLOROBENZENE-D5 21.71 117 1307729 5.00 ug/L 0.00 52) 1,4-DICHLOROBENZENE-D4 26.90 152 678212 5.00 ug/L 0.02

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.29 65 669337 5.91 ug/L 0.00 Spiked Amount 5.000 Recovery = 118.20% 3) 4-BROMOFLUOROBENZENE 24.30 174 570761 5.14 ug/L 0.00 Spiked Amount 5.000 Recovery = 102.80% 25) TOLUENE-D8 18.41 98 1638780 5.17 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.40%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.83 85 404138 8.90 ug/L 99 5) CHLOROMETHANE 5.42 50 525405 9.69 ug/L 99 6) VINYL CHLORIDE 5.57 62 403102 17.41 ug/L 100 7) BROMOMETHANE 6.54 94 357133 10.95 ug/L 97 8) CHLOROETHANE 6.69 64 363230 10.78 ug/L 99 9) TRICHLOROFLUOROMETHANE 7.25 101 696294 10.17 ug/L 99 11) l,l,2-Trichloro-l,2,2-trif 8.14 101 8425 0.28 ug/L 90 12) ACETONE 8.21 43 300170 32.30 ug/L 100 13) 1,1-DICHLOROETHENE 8.56 61 851244 10.37 ug/L 94 14) METHYLENE CHLORIDE 9.57 49 717746 9.84 ug/L 96 15) METHYL TERT BUTYL ETHER 9.88 73 610058 8.28 ug/L 99 16) TRANS-1,2-DICHLOROETHENE 10.23 61 824557 10.00 ug/L 94 17) 1,1-DICHLOROETHANE 11.12 63 928155 9.82 ug/L 97 18) 2-BUTANONE (MEK) 11.95 43 342682 33.92 ug/L 99 19) 2,2-DICHLOROPROPANE 12.34 77 697957 9.39 ug/L 95 20) CIS-1,2-DICHLOROETHENE 12.43 96 517930 9.33 ug/L 94 21) CHLOROFORM 12.77 83 •1023082 ■10.01 ug/L 98 22) BROMOCHLOROMETHANE 13.14 49 407358 9.60 ug/L 87 23) 1,2-DICHLOROETHANE 14.49 62 729537 10.33 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.67 97 792249 10.73 ug/L 99 27) 1,1-DICHLOROPROPENE 14.00 75 708432 10.43 ug/L 97 28) CARBON TETRACHLORIDE 14.25 117 690087 10.85 ug/L 97 29) BENZENE 14.59 78 1706598 10.09 ug/L 100 30) TRICHLOROETHENE 15.87 95 541682 10.25 ug/L 98 31) 1,2-DICHLOROPROPANE 16.23 63 429036 9.71 ug/L 99 3 2) DIBROMOMETHANE 16.89 174 255358 10.20 ug/L 97 33) BROMODICHLOROMETHANE 16.74 83 693022 10.36 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.21 63 157330 8.38 ug/L 99 35) METHYL ISO-BUTYL KETONE 17.30 58 288325 38.23 ug/L 92 36) CIS-1,3-DICHLOROPROPENE 17.83 75 608154 9.50 ug/L 98 37) TOLUENE 18.59 91 1796788 9.91 ug/L 100 38) TRANS-1,3-DICHLOROPROPENE. 18.86 75 453971 9.61 ug/L 97 39) 1,1,2-TRICHLOROETHANE 19.26 97 277675 9.28 ug/L 97 40) TETRACHLOROETHENE 20.04 166, 552781 10.30 ug/L 97 41) 1,3-DICHLOROPROPANE 19.78 76 529928 9.61 ug/L 99 42) DIBROMOCHLOROMETHANE 20.47 129 380521 9.85 ug/L 98 43) 1,2-DIBROMOETHANE 20.92 107 281550 9.23 ug/L 99 44) CHLOROBENZENE 21.79 112 1166005 9.55 ug/L 95 45) 1,1,1,2-TETRACHLOROETH7\NE 21.84 131 430836 10.00 ug/L 98 46) 2-HEXANONE 19.14 43 528689 37.87 ug/L 91 47) ETHYLBENZENE 21.84 91 2150127 10.20 ug/L 99

(#) = qualifier out of range (m) = manual integration 0408C10A.D HP031802.M Mon Apr 08 19:50:37 2002 Page 1

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