Volatile organic compound analysis results, sample AE07502, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02apr03\0403R5.D Vial: 3 Acq On 3 Apr 2002 10:17 am Operator: 201-wb Sample ref 5 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 3 10:56 2002 Quant Results File: HP031802.RES

Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Mar 28 15:03:13 2002 Response via : Initial Calibration DataAcq Meth :. HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.12 114 745402 5.00 ug/L 0.07 24) CHLOROBENZENE-D5 21.79 117 633347 5.00 ug/L 0.09 52) 1,4-DICHLOROBENZENE-D4 26.97 152 306571 5.00 ug/L 0.09

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 332303 5.41 ug/L 0.07 Spiked Amount 5.000 Recovery = 108.20% 3) 4-BROMOFLUOROBENZENE 24.36 174 249263 4.14 ug/L 0.07 Spiked Amount 5.000 Recovery = 82.80% 25) TOLUENE-D8 18.47 98 858378 5.60 ug/L 0.07 Spiked Amount 5,000 Recovery = 112.00%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.88 85 136799 6.18 ug/L 96 5) CHLOROMETHANE 5.40 50 168348 6.36 ug/L 98 6) VINYL CHLORIDE 5.62 62 149350 7.93 ug/L 99 7) BROMOMETHANE 6.61 94 118582 6.70 ug/L 98 8) CHLOROETHANE 6.74 64 114618 6.27 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.30 101 236805 6.37 ug/L 98 12) ACETONE 8.28 43 29310 7.32 ug/L 97 13) 1,1-DICHLOROETHENE 8.63 61 251625 5.65 ug/L • 96 14) METHYLENE CHLORIDE 9.64 49 199322 5.04 ug/L 98 15) METHYL TERT BUTYL ETHER' 9.94 73 171139 4.28 ug/L 100 16) TRANS-1,2-DICHLOROETHENE 10.30 61 237071 5.30 ug/L 97 17) 1,1-DICHLOROETHANE 11.19 63 262002 5.11 ug/L 99 18) 2-BUTANONE (MEK) 12.02 43 24411 4.45 ug/L 96 .19) 2,2-DICHLOROPROPANE 12.41 77 218912 5.58 ug/L 96 20) CIS-1,2-DICHLOROETHENE ' 12.50 96 153517 5.10 ug/L 99 21) CHLOROFORM 12.84 83 296654 5.35 ug/L 99 22) BROMOCHLOROMETHANE 13.21 49 111405 4.84 ug/L 89 23) 1,2-DICHLOROETHANE 14.56 62 204908 5.35 ug/L 100 26) 1,1,1-TRICHLOROETHANE 13.72 97 244067 6.82 ug/L 97 27) 1,1-DICHLOROPROPENE 14.05 75 212533 6.46 ug/L 97 28) CARBON TETRACHLORIDE 14.32 117 214384 6.96 ug/L 99 29) BENZENE 14.66 78 487599 5.95 ug/L 96 30) TRICHLOROETHENE 15.94 95 160579 6.27 ug/L 98 31) 1,2-DICHLOROPROPANE 16.29 63 122382 5.72 ug/L 99 32) DIBROMOMETHANE 16.96 174 62772 5.18 ug/L 97 33) BROMODICHLOROMETHTUSIE 16.81 83 195513 6.04 ug/L 94 34) 2-CHLOROETHYL VINYL ETHER 17.28 63 32871 3.85 ug/L 96 35) METHYL ISO-BUTYL KETONE 17.37 58 15024 4.11 ug/L 99 36) CIS-1,3-DICHLOROPROPENE 17.89 75 165145 5.32 ug/L 97 37) TOLUENE 18.66 91 521524 5.94 ug/L 100 38) TRANS-1,3-DICHLOROPROPENE 18.93 75 130973 5.72 ug/L 95 39) 1,1,2-TRICHLOROETHANE 19.33 97 76182 5.26 ug/L 95 40) TETRACHLOROETHENE 20.11 166 157934 6.08 ug/L 98 41) 1,3-DICHLOROPROPANE 19.85 76 140388 5.26 ug/L 98 42) DIBROMOCHLOROMETH7UJE 20.53 129 102718 5.49 ug/L 95 43) 1,2-DIBROMOETHANE 20.99 107 75239 5.09 ug/L , 98 44) CHLOROBENZENE 21.88 112 328720 5.56 ug/L 89 45) 1,1,1,2-TETRACHLOROETHANE 21.91 131 124802 5.98 ug/L 98 46) 2-HEXANONE 19.22 43 32389 4.79 ug/L 95 47) ETHYLBENZENE 21.91 91 632475 6.20 ug/L 98 48) P & M-XYLENE 22.07 106 418619 12.03 ug/L 85

(#) = qualifier out of range (m) = manual integration 0403R5.D HP031802.M Wed Apr 03 10:56:11 2002 Page 1

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