Volatile organic compounds analysis results, March 25, 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02mar25\0325R5A.D Vial 4 Acq On 25 Mar 2002 4:53 pm Operator 201-wb Sample ref 5 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 25 17:31 2002 Quant Results File: HP031802.RES

Quant Method C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Last Update Fri Mar 22 14:32:26 2002 Response via Initial Calibration . DataAcq Meth HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.03 114 1223057 5.00 ug/L -0.02 24) CHLOROBENZENE-D5 21.69 117 1126945 5.00 ug/L -0.02 52) 1,4-DICHLOROBENZENE-D4 26.87 152 625049 5.00 ug/L -0.02

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.27 65 554383 '5.50 ug/L -0’. 02 Spiked Amount 5.000 Recovery = 110.00% 3) 4-BROMOFLUOROBENZENE 24.28 174 502143 5.08 ug/L -0.02 Spiked Amount 5.000 Recovery = 101.60% 25) TOLUENE-D8 18.39 98 1421194 • 5.21 ug/L -0.02 Spiked Amount 5.000 Recovery = 104.20%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.82 85 171560 4.72 ug/L 99 5) CHLOROMETHANE 5.42 50 197527 458 ug/L 100 6) VINYL CHLORIDE 5.56 62 183440 _. . .78 g/L 98 7) BROMOMETHANE 6.53 94 138063 4.76 ug/L 96 8) CHLOROETHANE 6.66 64 137964 4.60 ug/L 96. 9) TRICHLOROFLUOROMETHANE 7.22 101 285679 4.69 ug/L 95 12) ACETONE 8.19 43 37565 1.26 ug/L 91 13) 1,1-DICHLOROETHENE 8.53 61 291085 3.98 ug/L 98 14) METHYLENE CHLORIDE 9.53 49 254499 3.92 ug/L 99 15) METHYL TERT BUTYL ETHER 9.86 73 260170 3.96 ug/L 99 16) TRANS-1,2-DICHLOROETHENE 10.20 61 281590 3.84 ug/L 96 17) 1,1-DICHLOROETHANE 11.10 63 334335 3.97 ug/L 98 18) 2-BUTANONE (MEK) 11.94 43 29586 ■ 3.29 ug/L s 92 19) 2,2-DICHLOROPROPANE 12.31 77 283767 4.45 ug/L 97 20) CIS-1,2-DICHLOROETHENE 12.41 96 200818 4.06 ug/L 97 21) CHLOROFORM 12.74 83 410888 4.52 ug/L 98 2 2) BROMOCHLOROMETHANE 13.13 49 143577 3.80 ug/L 88 23) 1,2-DICHLOROETHANE 14.47 62 302043 4.80 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.64 97 326933 5.14 ug/L 98 27) 1,1-DICHLOROPROPENE 13.96 75 259431 4.43 ug/L 99 28). CARBON TETRACHLORIDE 14.22 117 295095 5.39 ug/L 98 29) BENZENE 14.56 78 635810 4.36 ug/L 98 30) TRICHLOROETHENE 15.83 95 212113 4.66 ug/L 98 31) 1,2-DICHLOROPROPANE 16.19 63 157746 4.14 ug/L 93 32) DIBROMOMETHANE 16.86 174 106960 4.96 ug/L 99 33) BROMODICHLOROMETHANE 16.70 83 290296 504 ug/L 100 ■ 34) 2-CHLOROETHYL VINYL ETHER 35) METHYL ISO-BUTYL KETONE 17.20 17.28 63 58 49181 22387 3.23 ug/L 3.44 ug/L 92 75 36) CIS-1,3-DICHLOROPROPENE 17.81 75 233205 4.23 ug/L 98 37) TOLUENE 18.56 91 720088 4.61 ug/L 98 38) TRANS-1,3-DICHLOROPROPENE 18.83 75 197856 4.85 ug/L 96 39) 1', 1,2 -TRICHLOROETHANE 19.22 97 122926 4.77 ug/L 91 4 0) TETRACHLOROETHENE 20.01 166 233442 5.05 ug/L 98 41) 1,3-DICHLOROPROPANE 19.75 76 207291 4.36 ug/L 95 42) DIBROMOCHLOROMETHANE 20.45 129 169891 5.10 ug/L 93 43) 1,2 -DIBROMOETHANE 20.89 107 120851' 4.60 ug/L 92 44) CHLOROBENZENE 21.78 112 496320 4.72 ug/L 98 45) 1,1,1,2-TETRACHLOROETHANE 21.83 131 193395 5.21 ug/L 95 46) 2-HEXANONE 19.12 43 41624 3.46 ug/L 91 47) ETHYLBENZENE 21.81 91 881629 4.85 ug/L 98 48) P & M-XYLENE 21.96 106 582229 9.40 ug/L 89 (#) = qualifier out of range (m) = manual integration 0325R5A.D HP031802.M Mon Mar 25 17:31:55 2002 Page 1

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