Volatile organic compound analysis results, sample AE07376, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02apr01\0401C10.D Vial: 2 Acq On 1 Apr 2002 10:09 am Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 1 10:47 2002 Quant Results File: HP031802.RES

Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Mar 28 15:03:13 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.12 114 1266272 5.00 ug/L 0.07 24) CHLOROBENZENE-D5 21.78 117 1257577 5.00 ug/L 0.07 52) 1,4-DICHLOROBENZENE-D4 26.97 152 594370 5.00 ug/L 0.09

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 586384 5.62 ug/L 0.07 Spiked Amount 5.000 Recovery = 112.40% 3) 4-BROMOFLUOROBENZENE 24.38 174 503042 4.92 ug/L 0.09 Spiked Amount 5.000 Recovery = 98.40% 25) TOLUENE-D8 18.47 98 1511219 4.96 ug/L 0.07 Spiked Amount 5.000 Recovery = 99.20%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.86 85 575379 15.30 ug/L 97 5) CHLOROMETHANE 5.47 50 526590 11.61 ug/L 98 6) VINYL CHLORIDE 5.60 62 453895 14.18 ug/L 97 7) BROMOMETHANE 6.59 94 221016 7.35 ug/L 98 8) CHLOROETHANE 6.73 64 368579 11.87 ug/L 96 9) TRICHLOROFLUOROMETHANE 7.30 101 795672 12.61 ug/L 94 11) l,l,2-Trichloro-l,2,2-trif 8.17 101 10352 0.37 ug/L 86 12) ACETONE 8.26 43 303276 44.61 ug/L 97 13) 1,1-DICHLOROETHENE 8.62 61 833147 11.01 ug/L 98 14) METHYLENE CHLORIDE 9.62 49 631531 9.39 ug/L 99 ' 15) METHYL TERT BUTYL ETHER 9.93 73 599960 8.83 ug/L 99 16) TRANS-1,2-DICHLOROETHENE 10.28 61 749151 9.86 ug/L 97 17) 1,1-DICHLOROETHANE 11.19 63 829120 9.52 ug/L 97 18) 2-BUTANONE (MEK) 12.00 43 310192 33.31 ug/L 98 19) 2,2-DICHLOROPROP7VIE 12.39 77 740043 10.85 ug/L 94 20) CIS-1,2-DICHLOROETHENE 12.50 96 486658 9.51 ug/L 99 21) CHLOROFORM 12.82 83 948656 10.07 ug/L 99 22) BROMOCHLOROMETHANE 13.21 49 346637 8.87 ug/L 95 23) 1,2-DICHLOROETHANE 14.56 62 672521 10.33 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.72 97 797197 11.22 ug/L 99 27) 1,1-DICHLOROPROPENE 14.05 75 666524 10.21 ug/L 97 28) CARBON TETRACHLORIDE 14.30 117 711928 11.64 ug/L 98 29) BENZENE 14.64 78 1514198 9.31 ug/L 99 3 0) TRICHLOROETHENE 15.92 95 497182 9.78 ug/L 96 31) 1,2-DICHLOROPROPANE 16.28 63 377941 8.90 ug/L 99 32) DIBROMOMETHANE 16.96 174 228712 9.50 ug/L 95 33) BROMODICHLOROMETHANE 16.80 83 650853 10.12 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.28 63 142326 8.40 ug/L 99 35) METHYL ISO-BUTYL KETONE 17.35 58 253695 34.98 ug/L 89 36) CIS-1,3-DICHLOROPROPENE 17.89 75 559457 9.08 ug/L 99 37) TOLUENE 18.64 91 1602913 9.20 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.93 75 431350 9.49 ug/L 97 39) 1,1,2-TRICHLOROETHANE 19.31 97 251866 8.76 ug/L 97 40) TETRACHLOROETHENE 20.11 166 501845 9.73 ug/L 97 41) 1,3-DICHLOROPROPANE 19.85 76 ■466130 8.79 ug/L 98 42) DIBROMOCHLOROMETHANE 20.53 129 355141 9.56 ug/L 100 43) 1,2-DIBROMOETHANE 20.99 107 261891 8.92 ug/L 96 44) CHLOROBENZENE 21.86 112 1031992 8.79 ug/L 94 45) 1,1,1,2-TETRACHLOROETHANE 21.91 131 398816 9.62 ug/L 97 46) 2-HEXANONE 19.20 43 482065 35.91 ug/L 93 4 7) ETHYLBENZENE 21.91 91 1905898 9.40 ug/L 98

(#) = qualifier out of range (m) = manual integration 0401C10.D HP031802.M Mon Apr 01 10:47:55 2002 Page 1

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