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GC/MS calibration report, Nov 6 2001

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Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.

NYC-WTC_000069271–000069279

Folder label: “GCMS Scan X 10/22/01 An 11/8/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File ; C:\HPCHEM\1\DATA\NOV2601\LB.D Vial: 8 Acq On : 26 Nov 2001 5:32 pm Operator; 209 GALOS Sample : 10/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; RTEINT.P Quant Time: Nov 26 18:20 2001 Quant Results File: NP103001.RES Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ; Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth ; NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 28) Naphthalene 15.35 128 871 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 38) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. 40) Acenaphthylene 20.10 152 105 N.D. 41) Acenaphthene 20.65 153 209 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 21.03 65 1289 N.D. 44) 2,4-Dinitrotoluene 21.22 165 109 N.D. 45) Diethylphthalate 22.08 149 1165 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 22.69 77 185 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 55) Phenanthrene 25.06 178 1040 N.D. 56) Anthracene 25.21 178 1041 N.D. 57) Di-n-butylphthalate 27.00 149 8761 N.D. 5 8) Fluoranthene 28.68 202 1397 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 0.00 184 0 N.D. 63) Pyrene 29.35 202 1903 N.D. 64) Butylbenzylphthalate 31.51 149 2311 N.D. 65) Benzo(a)anthracene 32.98 228 15535 N.D. 66) Bis(2-ethylhexyl)phthalate 33.31 149 11597 N.D. 67) Chrysene 33.10 228 14328 N.D. 69) Di-n-Octylphthalate 35.04 149 9227 N.D. 70) Benzo(b)fluoranthene 36.12 252 13973 N.D. (#) = qualifier out of range (m) = manual integration LB.D NP112601.M Tue Nov 27 09:24:58 2001 Page 2

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