NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
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GC/MS calibration report, Nov 6 2001
Machine-extracted title · confidence 95%Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
NYC-WTC_000069271–000069279Folder label: “GCMS Scan X 10/22/01 An 11/8/01”
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NYC 9/11 Public Portal Document
'uantitation Report (QT Reviewed) Data File : C;\HPCHEM^MDATA\NOV2 6 01 \LB . D Vial: 8 Acq On : 26 Nd Operator: 2 09 G7VLOS Sample : 10/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 26 18:20 2001 Quant Results File: NP103001.RES Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.68 152 1328782 20.00 ug/1 -0.04 19) Naphthalene-d8 15.30 136 5148752 20.00 ug/1 -0.03 31) Acenaphthene-dlO 20.58 164 2527388 20.00 ug/1 -0.03 49) Phenanthrene-dlO 24.99 188 3603739 20.00 ug/1 -0.04 59) Chrysene-dl2 33.03 240 1961483 20.00 ug/1 -0.04 68) Perylene-dl2 37.12 264 1403367 20.00 ug/1 -0.04 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 10.45 99 240 0.00 ug/1 -0.54 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.69 132 877 0.01 ug/1 0.45 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.21 152 16348 0.27 ug/1 -0.04 Spiked Amount 50.000 Recovery = 0.54% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.60 172 430 0.00 ug/1 -0.02 Spiked Amount 50.000 Recovery = 0.00% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 29.91 244 858 0.01 ug/1 -0.04 Spiked Amount 50.000 Recovery = 0.02% Target Compounds Qvalue 2) Pyridine 5.19 79 475 N.D. 3) N-nitroso-dimethyl amine 5.16 74 936 N.D. 8) Phenol 11.06 94 428 N.D. 9) bis(2-Chloroethyl)ether 10.98 93 430 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 13.67 77 174 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LB.D NP112601.M Tue Nov 27 09:24:53 2001 Page 1
NYC-WTC_000069271
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