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GCMS analysis results for sample AD24698, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24698 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068853–000068865

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24698.D Vial: 19 Acq On : 6 Nov 2001 5:31 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.52 ug/1 81998 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-Da/ailorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benz^e-l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 45 3 BinJienylene 152 C12H8 000259-79-0 9 4^^ zenebutanoic acid, 3-nitro-.gamm 223 C10H9NO5i 006328-00-3 9 Abundance Scan 711 (11.570 min): 24698.D (-) pm/z 149.90 100.00% 1$0

5000 115 52 78 I®/" 11.2) 11.40 U.K) 11,80 I I I . , I T. I , , 1 . I ■ . . . I , ■ m/z 151.9069.31% nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Njundance i!©593; 1,4-Dichloroben2ene-d4 1$0

5000 52 78 115 11 20 11.40 11.60 11.80 m/z 114.90 a 37.79%

fn/z-> 30 35 40 50 UUn 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2.3,4-44-, 5,6-dichloro- 1!i0

115 5000 52 78 m/z 5270^^ 19.85%

35 87 I I ' I ' 11' ‘' 1' nn/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67017: Biphenylene 1!2 11.20 11.40 11.60 11.80 m/z78705 19.54% 5000

63 76 126 ................. Ill...... i ‘ 1 ‘ ‘' 1' 97 -’Yr ' I ' ‘ ' I ' ■ ■ ' m/z-> 30 40 50 60 70 )80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

24698.D NP103001.M Tue Nov 13 12:06:54 2001 Page 4

NYC-WTC_000068864

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NYC-WTC_000068864Source: NYC Law Department, mirrored locally

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