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GCMS analysis results for sample AD24472, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24472 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068432–000068446

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068445
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU~1\209\DATA\OCT1601\24472.D Vial: 17 Acq On : 17 Oct 2001 5:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.52 ug/1 50477 1,4-Dichlorobenzene-d4 11.77

Hit# Of 5 'entative ID MW MolForm CAS# Qual

1 1,4-Dic^orobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzenamine, 2-methyl-4-nitro- 152 C7H8N2O2! 000099-52-5 27 3 Ben^4namine, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 22 4 Bdnzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 17 Abundance Scan 717 (11.620 min); 24472.D (-) m/z 149.90 100.00% 1!i0

5000 115 78 I ' ' ' ' I ' i rr-f-T-i / I 52 40 11.20 11.40 11.60 11.80 12.00 tX m/z 151.90 63.54% ■nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 ...... .J,.... 11.20 11.40 11.60 11.80 12.00 52 78 m/z 115.00 37.38% 35 ........................ ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nttro- 77 106 152

11.20 11.40 11.60 11.80 12.00 5000 51 94 m/z78.05 a 20.75% 66 ' ' I ' ' ' ' I ' ' ‘ ' I .. I... ' 1 ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' I ' m/z-> 30 40 50 60 70 80 90 110 120 130 140 150 160 Abundance #66885: Benzenamine, 2-methyl-5-nitro- 77 106 152 11.^ 11.40 11.60 11.80 12.00 ~m7z 52.00 14774%

5000 51 94

' ' I ' ' ' ' I ' ' ' ' I ' ' OT ' ' 70 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' 1 ' ' ' ' I \oo 110 '' I ' I ' ' ' ' I ' ‘ ' ' I ‘ ' mfe-> 30 40 50 80 90 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24472.D NP103001.M Fri Nov 09 11:44:53 2001 Page 6

NYC-WTC_000068445

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NYC-WTC_000068445Source: NYC Law Department, mirrored locally

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