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← Document results/DEP Box 60/508 GCMS Scan X 10/11/01 An 11/2/01
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GCMS analysis results for sample AD24395, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24395 with detection of unknown compounds.

NYC-WTC_000068266–000068280

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068277
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24395.D Vial: 12 Acq On : 2 Nov 2001 1:46 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 11.57 0.54 ug/1 78893 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlor^>dnzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-1^^2<3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 32 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 2-Methyl-6-nitroaniline____________ 152 C7H8N2O2 000570-24-1 9 Abundance Scan 711 (11.574 min): 24395.D (-) Tm/z 149.90 100.00%

JL_ 1!i0

5000 115 78 ■n" *=r 40 .......... Jii............. 11.20 11.40 11.60 11.80 12.00 m/z 151.90 66733% m/z-> 30 40 50 60 70 80 100 110 120 130 140 150 160 Abundance #9593:1.4-DichIorobenzene-d4 1ii0

5000 115 1'1!^' '11'40' 'i7eo 11.80 '1'2'00 52 78 m/z 114.90 40.79% 35 I ‘ ‘ ‘ ‘ I tnfe-> ' M " 40 " M 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-<lichIoro- 1!i0

115 H.2!0 '1'1'40 11.^ I'tsb 12'00 5CMX) 52 78 m/z 78.05 21.53%

35 87 I I ' ! * ‘ ‘ ' 1 ‘ I I I ' ‘ • I ' mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- ' ‘ I ' 1ii2 11.20 11.40 11.60 11.80 12.00 m/z 52.00 17.52% 106 5000 53 81

TyT-rT-ryT-rT-rq[^L-T-TjT-rT-ryT-rl^ 92 122 136 tt+’ ■ I'''' I'''' I '' I ' ' I ‘ ‘ ' I ' ‘ ‘ ‘ I ' ' m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24395.D NP103001.M Wed Nov 07 14:31:19 2001 Page 3 NYC-WTC_000068277

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NYC-WTC_000068277Source: NYC Law Department, mirrored locally

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