GCMS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\LBA.D Vial: 8 Acq On : 1 Nov 2001 9:51 pm Operator: 209 GALOS Sample : 10/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.67 ug/1 97109 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 91 2 2-Hexanene, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 78 3 Methyx Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 2-Hexanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2! 061141-74-0 45 Abundance Scan 150 (6.421 min): LBA.D (-) Tm/z 42795 100.00% 43

58

jy 5000

100 6.00 6.20 6.40 6.60 6.80 ..... ................ . lOOIIOIMI^I^ m/z 58.00 64.07% ■n/z-> 20 30 40 50 60 70 80 90 Abundance #63387:2-Hexanone 43

58 5000j 6.00 ‘eio 6.40 6.60 6.80 100 m/z m/z41:0517.29% 71 85 ■ I ■ • I • I ■ ■ ■ ''i I I 1 Tife-> 20 30 40 ' I ' ' ‘ 50 60 I ' SZZ^ZZZ ZZ Z ZiSZimZw ot im iio Abundance #11968:2-Hexanone, 4-hydroxy-3-propyi- 40 58 6.00 6.^’ 6.^ 6.^' 5000 29 m/z 57.00 16.27%

Tife-> Abundance u 20 30 ' 11' ■ ‘ 1 ‘ 40

43 50 60 70 71 85 ....80........ ^4^ 100 140 90 100 110 'iM' iM' '146 #63350: Methyl Isobutyl Ketone 6.00 6.20 6.40 6.60 6.80 m/z 100.05 137^8% 5000 58

85 100 27 I . 67 I I I I • 'rI’l I 1 « « j I I I I I r 1'1 1 j 1

TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60 6.80

LBA.D NP103001.M Wed Nov 07 14:58:10 2001 Page 1

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