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GCMS analysis results for sample AD24694, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24694 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068696–000068707

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068704
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24694.D Vial: 7 Acq On : 5 Nov 2001 5:49 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.58 ug/1 106216 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hex, me 100 C6H120 000591-78-6 91 2 2-Hl 'anone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Ml lyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 -Hexanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2! _______ 061A41-74-0 53 Abundance Scan 151 (6.428 min): 24694.D (-) m/z 42.95 100.00% 40

58 5000

71 85 100 6.00 6.20 6.40 6.60 6.80 ,51 I T ...... Jit, I , , , I l , ............ I I I i-p. m/z 58.05 53773% 'p'''p Ti&-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63387: 2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 100 m7z 41705 18.37% 71 85 i I .... . m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.00 6.20 6.40 6.60 6.80 5000 29 "mTz 57700 14.65%

' I ' ' ' ' I ' '' I 11 T-p-r^ ,1 y 85 100 140 rTi/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63354: Methyl Isobutyl Ketone 43 6.00 6.20 6.40 6.60 6.80 m/z 99.95 12.03%

5000

mfe-> 20 30 40 50 58

60 70 80 85

90 100

100 110 120 130 140 6.00 1 6.20 6.40 6.60 6.80

24694.D NP103001.M Fri Nov 09 12:16:53 2001 Page 1

NYC-WTC_000068704

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NYC-WTC_000068704Source: NYC Law Department, mirrored locally

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