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GCMS analysis results for sample AD24220, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24220 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068055–000068069

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24219.D Vial: 6 Acq On : 1 Nov 2001 7:54 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 l,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.57 ug/1 82120 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-D ;hlorobenzene - d4 150 C6C12D4 003855-82-1 53 2 Benz .e-l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 2-Ml hyl-6-nitroaniline 152 C7H8N2O2 000570-24-1 10 4 Be: aldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 ^bundan^ Scan 711 (11.575 min); 24219.D (-) m/z 149.90 100.00% 150

5000 115 52 78 11.20 11.40 11.60 11.80 12.00 p4^ 1''' ‘ I m/z 151.90 57.52% ttZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 1$0

5000 115 I I I . I . I . . i 1-f, 1 . . I ,

78 1120 11.40 11.60 11.80 12.00 52 m/z 114.90 36.56%

T,Zz-> 20 30 35 40 XnJrX - 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1.2,3.4-d4-, 5,6-clichloro- 150 T 115 11.20 11.40 11.60 11.80 12.00 5£X)0 52 78 m/z 78705 19727%

35 87 I ■ I ■ • ■ • I • ■ I • 1 ■• • • I • T rfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66883; 2-Methyl-6-nitroaniline 77 1$2 1120 11.40 11.60 11.80 12.00 m/z 52.00 15.89%

5000 106 52 94 122 T-p-TT-r-p- 11' ' n'' *' ‘ I T ''“m' ■nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.2) 11.40 11.60 11.80 12.00

24219.D NP103001.M Tue Nov 06 11:50:02 2001 Page 4

NYC-WTC_000068066

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NYC-WTC_000068066Source: NYC Law Department, mirrored locally

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