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GCMS analysis results for sample AD24220, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24220 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068055–000068069

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068067
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0101\24219.D Vial: 6 Acq On 1 Nov 2001 7:54 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,2-Benzenedicarboxylic acid. Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 41.59 0.64 ug/1 90506 Perylene-dl2 37.15 Hit# of 5 Tahtative ID MW MolForm CAS# Qual 1 1,2-Benzen^icarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 12 2 Mercaptoaz^etic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 12 3 SilanamiZe, N-[2,6-dimethyl-4-[(tri 281 C14H27N0Si2 072088-09-6 11 4 3-Isopp6poxy-l, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 9 Abundance Scan 3981 (41.594 min): 24219.D (-) m/z 73.00 100.00% 147

5000 221

■nZz-> Abundance 96 193 40 K) 80 100120140160180200220240260280300320340360380400420 #72973:1,2-Benzenedicarboxylic acid, bis(trimethyisilyl) e 281 J., 429 41 T 41.40 41.60 41.80 42.00 m/z 147.00 68784%

147 73 5000 41 Im' '4114b' 4ileo‘ 4'1 lab' '42.(» 45 295 m/z 221.00 48.01% 119 , yTTTrpTTTpTTTpTTTyrnTyrTTTyrTT^ Ttfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #30949: Mercaptoacetic add. bis(trimethylsilyl)- 73 147 41.20 41.40 41 .M 41.80 42.00 5000 m/z 354.95247^7% 221 45 104 I Tife-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #39584: Silanamine, N-[2,6-dimettiyl-4-[(trimethylsilyi)oxy] 7(3 41 .M 41.40 41.60 41.80 42.00 281 m/z 147.90 17707% 209 5000 45 251 dzv 179 TTj)TTTJTTiTrTTTpTTr)4rTTp7^ I '1 . , . . I I I I .'I , , A ■ . I . ■ ■ ■ I I I . . , . . . . I . , . , I ■ . ■ , I > ■ . ■ I I I t I , . I I I I

Tife-> 40 60 80 1001201401601802(K)220240260280300320340360380400420 41 lab' 4114b' 41^60 41 Im '4200’

24219.D NP103001.M Tue Nov 06 11:50:04 2001 Page 5

NYC-WTC_000068067

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NYC-WTC_000068067Source: NYC Law Department, mirrored locally

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