GCMS analysis results for sample AD24217, Nov 6 2001

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Library Search Compound Report Data.File : C:\HPCHEM\1\DATA\NOV0101\24216.D Vial: 3 Acq On : 1 Nov 2001 4:58 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.41 0.60 ug/1 100243 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hex: •ne 100 C6H12O 000591-78-6 91 2 Oxir fe, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 78 3 2-Hl :anone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 Ml lyl Isobutyl Ketone_____________ 100 C6H12O 000108-10-1 50 Scan 149 (6.414 min): 24216.D (-) m/z 43.00 100.00% 43

58 5000

100 6.^ " R46 ” fteo " 6.80' 51 l-i-rp- I. 71 ' I ' ' ' ' I ‘ I 85 I ' I ' ’ ‘ ‘1 ’ 6.00 inTz 58.00 55.59% TiZz-> 20 30 40 50 60 70 80 90 1OT110lSl30140 Abundance #1556:2-Hexanone 43

58 I I I I Vv. 7| I I I I . 5000 6.00 6.20 6.40 6.60 6.80 m/^ 56.95 18.91% 27 71 85 100 ........ I A-*' ' I ‘ ‘ ■ I ' ■ ' ' I ' ■ ' ' I ' Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1530: Oxirane. 2-methyl-2-(1-methyIethyl)- 43 58 6,00 6.20 6.40 6.60 6.80 5000 m/z 100.05 12.88% 71 J 30 85 100 • I • ■ ■ ■ I ■ ■ • ■ I • • • I • • • ■ I ■ ■ ■' I • Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968; 2-Hexanone. 4-hydroxy-3-propyl- 43 6.00 6.20 'e^o 6.60 6.80 58 m/z 41.00 12.77% 5000 29

hfife-> ,1, ' I ' ' ' ' I ■ ' ' ■ 1 I ■ • ‘ 1 • '' I' 20 30 40 50 60 71 85 T-fVr-rTq-rA-r-p-TT-rj-r-r-^^ 70 80 90 100

100 110 1» 130 140 140 6.00 6.20 6.40 6.60 6.80

24216.D NP103001.M Tue Nov 06 11:45:36 2001 Page 1

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