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GCMS analysis results for sample AD24217, Nov 6 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24217 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068003–000068021

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068011
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24216.D Vial: 3 Acq On : 1 Nov 2001 4:58 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.25 ug/1 208660 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pent ano: , 4-hydroxy-4-niethyl- 116 C6H12O2 000123-42-2 72 2 Acetic id, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Acetone 58 C3H6O 000067-64-1 9 4 Morpnoline, 4-methyl-___________ 101 C5H11N0 000109-02-4 9 Abundance Scan 288 (7.690 min): 24216.D (-) m/z 42.95 100.00% 40

5000 59

101 '7.46' 7.to' 7.^ ioo' nfe-> ‘ I ‘ 10 ' I ' 20 30 40 50 +-T nSUU 60 '70 " OT 69 83 I I M ' ' 100 ' ' ■ ■ I 110 m/z 59.05 49.57% Abundance #64274:2-Pentanone. 4-hydroxy-4-methyl- 40

5000 J 59 "7.^' 7.^' '7.^ 8.06' m/z 100.95 22.79% 27 101 03 ' 1 ‘ ‘ ‘ I ‘ ‘ ‘ 1 ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 4)3 T 7,40 7.60 7.80 8.00 5000 57 m/z 58.05 15.81%

mfe-> Abundance

5000 10 15 20 27 30 40 40 T^V-i-rT-i-r-r-T-rY-rT-rT-p-rT-ryT-r-r-r-i- 60 #94: Acetone 70 80 90 101

100 110 L ''7.^' 'zro '7.^' 'abo' " in/z 41.05 7761%

15 58 27 n-4 i-r-r-p I ' ‘ ' I ' ' ‘ ’ I ' ' ' ' 1 ' ' ■ ‘ I ' ' ' ' I ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

24216.D NP103001.M Tue Nov 06 11:45:38 2001 Page 2

NYC-WTC_000068011

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NYC-WTC_000068011Source: NYC Law Department, mirrored locally

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