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GCMS analysis results for sample AD24217, Nov 6 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24217 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068003–000068021

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\NOV0101\24216.D Vial: 3 Acq On : 1 Nov 2001 4:58 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 88213 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 •entative ID MW MolForm CAS# Qual 1 l,4-Dichl6robenzene-d4 150 C6C12D4 003855-82-1 38 2 BenzenQ^l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 27 3 4-Ami^-2-chlorobenzonitrile 152 C7H5C1N2! 020925-27-3 9 4 2-Methyl-6-nitroaniline___________ 152 C7H8N2O2i ____ 00057022421 9 Abundance Scan 711 (11.573 min): 24216.D (-) Fm/z 149.90 100.00% 1$0

5000 115

52 78 T n -- 7 87 1120 11.40 11.60 11.80 12.00 .1,, 63 ,1. '■ ''I' - m/z 151.90 67.04% Tl/z-> Abundance 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #9593:1,4-DichIorobenzene-d4 1!i0 ft 5000 115 78 1120 11.40 11.60 11.80 12.00 52 m/z 114.90 40.80% 35 44^ Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-. 5,Michloro- 1!i0 . I . I . . I ■ I ■ Tj t / . > ■ > > I I

115 1120 11.40 11.60 11.80 12.00 5000 52 78 m/z 78705 21.25%

87 35 A A I I ' I'''' I' ' I ' ' ' ‘ 1 ' I'''' I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10110:4-Aniino-2-chlorobenzonitrile 1ii2 1120 11.40 11.60 11.80 12.00 m/z 52.00 . 15.72% 5000

. ... ... r.. 30 40 50 60 70 80 90 117 125

100 110 120 130 140 150 160 r TT-p-T “r 11.20 11.40 11.60 11.80 12.00

24216.D NP103001.M Tue Nov 06 11:45:41 2001 Page 3

NYC-WTC_000068012

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NYC-WTC_000068012Source: NYC Law Department, mirrored locally

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