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GC/MS analysis results for sample AD23359, Oct 19 2001

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Laboratory report documenting GC/MS analysis of environmental sample AD23359 conducted on October 19, 2001.

NYC-WTC_000088636–000088647

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088644
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23359.D Vial: 8 Acq On : 18 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101 .M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.50 ug/1 47966 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-He3^none 100 C6H12O 000591-78-6 91 2 2-H^anone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 53 4 Oxirane, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 \bund^ce Scan 157 (6.486 min): 23359.D (-) “m/z 47795 100700% 43

58 5000

7 85 100 6.20 AJ 6.40 6.60 6.80 50 . I m/z ■n-|-rTV- 'i ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' 58.05 60.58% llZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

58 5000 6.20 6.40 6.60 6.80 m/z 41.05 17.66% 27 71 85 100 ' I ' ' ' ' I ' Tlfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968; 2-Hexanone, 4-hyclroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 29 m/z 577^00 16737%

71... 85.... ' I ' ' ' ' I ' ' ' ' I ' ill 140 Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63354: Methyl Isobutyl Ketone 43 6.20 6.40 6.60 6.80 m/z 100.05 11.98% 5000 58 85 100 67 I ............ I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

23359.D NP091101.M Fri Oct 19 10:14:45 2001 Page 1

NYC-WTC_000088644

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NYC-WTC_000088644Source: NYC Law Department, mirrored locally

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