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GCMS analysis results, sample AD23905, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23905 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067522–000067534

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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Scanned page image, NYC-WTC_000067530
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23905.D Vial: 10 Acq On : 17 Oct 2001 10:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method s C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.85 ug/1 82576 l,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanon^ 100 C6H12O 000591-78-6 91 2 Oxirane,-methyl-2-(1-methylethy1) 100 C6H12O 072221-03-5 64 3 Meth’ X Isobutyl Ketone 100 C6H12O 000108-10-1 58 4225^ :anone, 4 - hydroxy - 3 - p r opy 1 - 158 C9H18O2 062338-17-4 56 ^undarjefe Scan 158 (6.489 min): 23905.D (-) ra/z 42.95 100.00% 40

58 5000

71 85 100 6.20 6.40 6.60 6.80

xL ... . .. I r[bll|llll|llll|llll| m/z^ 58.05 54.37% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556:2-Hexanone

58 5000 6.20 6.40 6.60 6.80 m/z 41.00 18.09%

Uc 27 71 85 100

Tife-> I'l.... ...... .. t+-t 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4- Abundance #1530: Oxirane. 2-methyl-2-(1-m6thyiethyl)- <43 58 _Z6S_a^__6S_6S__ 5000 m/z 57.00 16.34% 71

30 66 85 1M

Tife-> 20:^30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63351: Methyl Isobutyi Ketone 40 6.^ 6.40 6.60 6.80 m/z 100.05 10.96% 5000 58 27 85 100

mto ' II ‘‘'' II ‘‘ I - I'' ‘‘ II" " ‘‘'' I1" " I l| I • • Il 11 ■ 11 > 1111" • > 1 ■ " ■ 1 "I < 11"

20 25 30 35 40 45 50 55 fin fiS 70 75 fin RS Of) f« inn IfK ■ 11111(1" 11II .11111 n *...... iV,>i»...... R9n R4n RRn rro

23905.D NP101901.M Tue Oct 23 12:51:50 2001 Page 1

NYC-WTC_000067530

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NYC-WTC_000067530Source: NYC Law Department, mirrored locally

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