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GCMS analysis results, sample AD23947, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23947 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067651–000067674

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT2301\23915.D vial: 19 Acq On : 24 Oct 2001 5:24 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.71 2.34 ug/1 364860 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 64 2 1,8 -Nonanediol-methyl - 174 C10H22O2! 054725-73-4 17 3 Morpholine, ^methyl- 101 C5H11N0 000109-02-4 9 4 5-Hexen-2-c e 98 C6H10O 000109-49-9 9 Abundance /' Scan ^1 (7.712 min): 23915.D (-) Wz 42.95 100.00% 43

59 5000

101 , I 109 126 7.40 7.a) 7.80 8.00 70 83 91 149 ■I. ... I ..4' 11 > • • • I rp-rrtftT-TTYTTTTpTT-p TT-p-T m/z 59.05 51729% 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #3245:2-Pentanone, 4-hydroxy-4-methyl- 4i3

50CX) 59 7.^' 7.60 ■ ■ I ■ i , I 7.80 8.00 m/z 101.05 19.22% 31 ■1.4. .... T.. ..... ttZz--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #16264:1.8-Nonanedjol, 8-methyl- 5)9 ‘ ‘ I ‘ ‘ ‘ I ' ' ' ‘ I ‘ ‘ ' I ‘ ‘ ‘ I 7.40 7.60 7.80 8.00 5000 m/z 58705 15.52%

83 98 123 t ' ■ ■ • • I ''' nft-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #1640: Morpholine, 4-methyl- ' n . I -I . I , I f. . I ,^<-1'1 r . 1 !-[ 43 7.40 7.60 7.80 8,00 m7z 41.05 8.86% 5000 101 71

Tlfe-> JLVr 10 20 30 40 I 50 70 I 80 90 f I'' ‘ ‘ I ‘ ‘ ‘' 1 ‘' I ‘ ‘ ‘' I 100 110 120 130 140 150 7.40 7.60 7.80 8.00

23915.D NP101901.M Thu Oct 25 12:12:01 2001 Page 6

NYC-WTC_000067667

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NYC-WTC_000067667Source: NYC Law Department, mirrored locally

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